简介:Thisreviewcoverstheprogressoflightscatteringapplicationsinthefieldofparticlecharacterizationinthepastdecade.Thereviewaddressesstaticlightscattering(themeasurementofscatteringintensitiesduetolight-particleinteractionatvariousspatiallocations),dynamiclightscattering(themeasurementofscatteringduetolight-particleinteractionasafunctionoftime),andscatteringtrackinganalysis(thetrackingofparticlemovementthroughscatteringmeasurement).
简介:Inthispaper,animagedynamiclightscatteringmethodfornanoparticlesizingisintroduced.ThespatialdistributionofthescatteredlightsfromnanoparticlesundergoingBrownianmotionwascapturedatahighframeratebyadigitalcamerawithinonesecond,whichisconsiderablyfasterthantheconventionalphotoncorrelationspectroscopymethod.Thecapturedseriesofphotographsweremeshedintothousandsofsmallunitsforcalculatingtheintensityautocorrelationfunctionsinparallel.Experimentalresultsfromthemeasurementsofthreereferencenanoparticlesamples(27,80,and352nmindiameters)demonstratedthefeasibilityofthismethod.
简介:Whenasurfaceisilluminatedbylaser,thefieldofdiffusingreflectivelightcanbedescribedbyFresnel-KirchhoffintegrationintheregionofFresnel.Ifthecorrelation,beforeandafterthechangeofintensityfield,isanalysedbystatisticalmethod,threegoverningequationsforvariationsofintensityfieldandspecklemovementformulascanbeobtained.Intheseequations,thesurfacemotion,deformationandwavelengthchangeareallconsideredtocausethespecklemovement.
简介:Thispaperpresentsamethodtomeasurethein-planedisplacementfieldsofcurvedsurfacebymoireinterferometryofpartialcoherentlight.Themethodhasthefollowingadvantages:simpleopticalsystem,norequirementonvibrationisolation,highsensitivity,largemeasuringrange,highcontrastofinterferencefringesandavailabilitytoin-situstructuraltesting.Thepresentpaperalsogivestheoreticalanalysisofthemethodandtheformulasoflightintensityanddisplacementfield,andintroducesareplicationtechniquetoformahighfrequencyreflectancegratingonthecurvedsurface.Theexperimentsachievedthemeasurementofthesurfacedisplacementfieldofacylindricalshell—thesimultaneouscircumferential,axialand45°displacementfields.Thetorsionaltestdataforsurfacedisplacementofacircularbaragreewellwiththetheoreticalresult.
简介:W,N共同做TiO2nanoparticles被一个solgel方法综合。准备样品被X光检查衍射(XRD)描绘,域排放扫描电子显微镜学(FE-SEM),传播电子显微镜学(TEM),Fourier变换红外线的光谱学(英尺红外),X光检查光电子光谱学(XPS)和弥漫的反射spectrophotometry(医生)。结果证明共同做的光催化剂是有22.5nm的最小的粒子尺寸的实质上一致的球形的粒子。比作未做的TiO2,N-TiO2和P-25,W的吸收边,N共同做转移到更长的波长的TiO2和它为在Xe灯(350W)下面的甲基橘子(瞬间)的降级的photocatalytic活动更高。
简介:TiO2-loadedactivatedcarbonfibers(ACF)werepreparedbyahydrothermalmethod.Thesampleswerecharacterizedbyscanningelectronmicroscopy(SEM),X-raydiffraction(XRD),Fouriertransforminfrared(FT1R)spectrometryandUV-visdiffusereflectancespectra(DRS).SEMimagesshowedthattheTiO2nanoparticlesweredepositedonthesurfaceofACF,andtheparticlesizeandloadingamountofTiO2werevariedbychangingtheinitialconcentrationoftetrabutyltitanate(TBOT).TheresultsofanashexperimentshowedthattheloadingamountsofTiO2were18.4%,43.3%,52.5%,75.1%,and91.1%forinitialconcentrationsofTBOTof0.07,014,0.21,0.28,and0.35mol/L,respectively.PhysicalinteractionsplayedanimportantroleintheformationofTiO2/ACFcompositefibersthatabsorbUVandvisiblelight.ComparedwiththoseofACF,improvedadsorptionandphotocatalyticactivitytowardRhodamineB(RhB)wereobservedforTiO2/ACFcompositefiber.TheRhodamineBcouldberemovedefficientlybyTiO2/ACFcompositefibers,andtheTiO2loadingamounthadasignificanteffectonthephotocatalyticactivityofTiO2/ACFcompositefibers.