摘要
Molybdenumoxidenanostructuredthinfilmsweregrownonfluorinedopedtinoxide(FTO),indiumdopedtinoxide(ITO)andordinaryglasssubstratesbythermalevaporationprocesswithoutvacuumandcatalystsusingmolybdenumtrioxide(MoO3)powderasasourcematerialandoxygenasacarriergas.Variousmorphologiesincludingnanobelts,disksandhexagonalrod-likenanostructureswereobtainedbychangingthesourceandsubstratetemperaturesduringthegrowthofMoO3thinfilms.Structuralparameters,morphology,compositionandsurfacefeaturesofthefilmswerecharacterizedbyXRD,SEM,EDAX,XPS,AFMandRamanspectroscopy.Thefilmswereorthorhombicinstructurewithpreferredorientationalong(010)plane.Morphologyanalysisrevealsrandomlyalignednanobeltswith40nminthicknessandawidthof800nmand3–12mminlength.Thediskshave1.5μmdiameters,1μmthicknessandhexagonalrod-likenanostructureswithalength,breathandwidthof2μm,1μmand100nmareformed.ThesampleswereinvestigatedunderdarkandphotocurrentconditionsinH2SO4aqueoussolutionasafunctionofappliedpotential.ThephotocurrentdensityofsamplespreparedonITOandFTOsubstratesampleswerecomparedandtheresultsarediscussed.
出版日期
2016年05月15日(中国期刊网平台首次上网日期,不代表论文的发表时间)