简介：铁矿石经浓盐酸和少量的SnCl2溶液加热到45℃溶解后,用SnCl2-TiCl3还原滴定Fe（Ⅲ）,使Fe（Ⅲ）还原为Fe（Ⅱ）,再以K2Cr2O7滴定全铁含量。本方法对实验操作温度,试样溶解酸的选择有一定的要求,宜选用非氧化性强酸在30-60℃溶解矿样。

简介：近来，钢板市场对建筑屋顶和外墙等功能性薄板需求在不断增大。JFE公司的镀锌和涂层产品已用于各种建筑以满足节能、防菌、防霉、防静电和抗热等性能的需求，JFE镀锌和涂层公司生产了各种涂层钢板。除了优秀的防菌和防霉产品PURE—CLEAN之外，还有能很好防止静电的CLEAN—ACE产品以及耐热产品BAKE—CLEAN。

简介：1前言在电炉炼钢生产过程中,使用涂层吹氧管代替非涂层吹氧管进行吹氧操作,可以减少吹氧管消耗、降低炼钢生产成本,提高经济效益,此项措施已在许多电炉钢厂广泛采用。鉴于此,我们分别于1993年上半年及1994年上半年在一炼钢厂和二炼钢厂采用涟钢振兴冶金材料厂生产的涂层吹氧管进行了试验,考察了涂层吹氧管的使用效果,现已全面推广使用,效果良好。

简介：Cr2O3-formingferriticstainlesssteelshavebeenwidelyexploredasintermediatetemperaturesolidoxidefuelcells（SOFCs）interconnects.However,theevaporationofchromiascalemightmigratetoandpoisonthecathode,leadingtodegradationofthecellperformance.Inthisstudy,Ni-Co-Fe-Pcoatingsweredepositedontheferriticstainlesssteelbymeansofacost-effectivetechniqueofelectrolessmethod.Theyareexpectedtobeconvertedinto（Ni,Co,Fe）3O4spinelwithahighelectricalconductivityandCTEmatchwithstainlesssteel,whichcanblocktheevaporationofchromiaformedonsteelsubstrateexposedtothecathodeenvironmentoftheSOFC.TheeffectsofpH,massratioofFeSO4/（FeSO4+NiSO4+CoSO4）andtemperatureofsolutiononthedepositionrate,compositions,surfacemorphologiesandstructuresoftheNi-Co-Fe-Pcoatingswereinvestigated.TheresultsindicatedthatthedepositionrateincreasedwithincreasingpHwhenpHwaslowerthan9andthenreducedwhenpHwashigherthan9.Thedepositionrateincreasedwithincreasingtemperaturewhentemperaturewaslowerthan80℃andthendecreasedwhentemperaturewashigherthan80℃.ThedepositionratedecreasedwiththeincreaseinmassratioofFeSO4/（NiSO4+CoSO4+FeSO4）.ThecoatingsconsistedofNi,Co,FeandP.Thephasestructureofthecoatingwasamorphous.

简介：ThehotductilityofFe-36NiinvaralloywithdifferentadditionsoftheelementceriumwasinvestigatedusingaGleeble-3800thermal-mechanicalsimulatoroverthetemperaturerange850-1050℃,andtheimprovementmechanismofthehotductilitywasanalyzedusingacombinationofSEM,EDS,andOM.TheresultsindicatedthatFe-36Niinvaralloyexhibitedpoorhotductilitybelow1050℃,whichwasmainlyattributedtoweakgrainboundariesandtheactionofgrainboundarysliding.However,thealloyswithceriumcontentsof0.016%and0.024%bothdemonstratedsubstantialimprovementinthehotductilityovertheentiretestingtemperaturerange.Theobservedimprovementofthehotductilityofthealloywith0.016%ceriumat950℃andthealloywith0.024%ceriumat900℃wasassociatedmainlywiththegrainboundarystrengtheningandtherestrictionofthegrainboundaryslidingbecausetheadditionofceriumreducedthesegregationofsulfuratgrainboundariesandrefinedthegrainstructure.Theoccurrenceandaccelerationofdynamicrecrystallizationwerefoundtoberesponsibleforthehighhotductilityofthealloywith0.016%ceriumat1000℃andthealloywith0.024%ceriumat950-1000℃asaresultoftherefinementofthegrainstructurebyadditionofcerium.

简介：TheeffectofCe,LaandmischmetalonthesolidificationstructureofFe-36Niinvaralloywasinvestigated.Theresultsshowthatgreatamountsofhigh-meltingpointcompounds(Ce2O3,La2O2Sand(Ce,La)2O2S)respectivelyformedinthealloywiththeadditionofCe,Laormischmetal.Basedonthetheoryoflatticemisfit,thelatticemisfitbetweenthe(0001)surfacesofCe2O3,Ce2O2SandLa2O2Sand(100)surfaceofFe-36Niinvaralloywere6.21%,5.77%and5.42%,respectively,whicharerelativelylow.Therefore,Ce2O3,La2O2Sand(Ce,La)2O2Scouldserveasthecoreofheterogeneousnucleation,improvetheequiaxedgrainratio,reducetheequiaxedgrainsizeandrefinethesolidificationstructureofalloy.

简介：碳钢薄板厂转炉一次除尘采用湿式法除尘,存在以下问题:1、转炉烟气中的灰尘、水汽和混合气体在风机作用下,形成高速气流,严重冲刷、侵蚀风机转子前后端板、叶片。2、转炉烟气中的灰尘附着在转子前盘、后盘和叶片表面,破坏转子动平衡,转子使用周期较短。"3、影响风机轴瓦、偶合器使用寿命,对风机基础也产生较大影响。4、转子在线使用周期短,检修时间长,人力物力消耗巨大,不利于设备管理和降低费用消耗。炼钢保障作业区相关技术人员针对转炉一次除尘风机转子工作特点和工作环境,进行了多方面分析、论证,在转子表面喷涂金属保护层、对转子反冲洗系统进行改进,降低了转子振动,延长了转子使用周期,缩短了检修时间和人力物力财力消耗,避免了转炉烟气中烟尘、水分及腐蚀性气体对转子及叶片表面的冲刷和侵蚀,延长转子使用寿命,提升了设备综合效益。

简介：Thehot-deformationbehaviorofFe-Mn-Ctwinninginducedplasticity(TWIP)steelwasinvestigatedbyconductinghotcompressiontestswithinarecommendedhotrollingtemperaturerangeatvariousstrainrates.Flowresistancecurvesduringhot-deformationwereobtained,andstrainratesensitivitiesandactivationenergiesforplasticdeformationwerecalculatedusingthepowerlaw.ItisfoundthattheadditionofAlandSiclearlyincreasesthepeakstressesforthepresentalloys,especiallyat950℃.ButMnhasaminoreffectonthestress-straincurvesandactivationenergywhenitscontentvariesfrom15mass%to22mass%forthepresentalloys.

简介：ItisfundamentallyimportanttounderstandtheinfluenceofstrainonthedensityofdeformationtwinsinTWIPsteelbecausetwinningisitsdominantdeformationmechanism.ThedeformationbehaviorofaFe-30Mn-4Si-3Al-0.097CsteelhasbeeninvestigatedbyX-raydiffraction(XRD),electronbackscatterdiffraction(EBSD)andtransmissionelectronmicroscopy(TEM)techniques.Samplewithanaveragegrainsizeof10μmwasdeformedincold-rollingwithareductionof10%,20%,30%,40%,50%,60%and70%,respectively.Themechanicalpropertiesofthecold-rolledsampleswerefurtherinvestigatedbytensiletests.Theyieldstrength(σy)andultimate-tensile-strength(σUTS)oftheas-preparedsampleis480MPaand850MPa,respectively.However,undercoldrollingdeformation,thetensilestrengthobviouslyincreaseswithanincreaseinrollingreduction.Thesamplewitharollingreductionof10%exhibitsσyof610MPaandσUTSof-1000MPa.Theyieldstrengthandtensilestrengtharefurtherenhancedupto1320MPaand1378MPaforthespecimenwitharollingreductionof70%,regardlessofthepoorductilityof6.7%.ThedeformationmicrostructureswerestudiedbyEBSDandTEMobservations.Itisfoundthat,withincreasingrollingreduction,theaveragedistancebetweendeformationtwinsdecreasesgraduallywhilethedensityofdeformationtwins(thelengthoftwinboundaryinunitarea)exhibitamaximumvalueat40%cold-rolling+tension.Carefullystatisticsanalysisrevealsgrainorientationiscloselyrelatedtothedeformationtwinsandtheunderlyingmechanismgoverningthetwinningisdiscussed.

简介：Resultspresentedinthisstudycontributetoinvestigationofthemicrostructureandmechanicalpropertiesofthehot-rolledFe16Mn0.6Csteelplates.Thesteelplateshavebeenproducedbybeinghot-rolledattemperaturesrangingfrom1100℃to850℃insevenpassesto97.5%reductioninthicknessandthencooledinafurnaceof650℃.Someplateshavebeenannealedattemperaturesrangingfrom300℃to1100℃for5minto60min,andthenfollowedbywaterquenching.Thereareannealingtwinsinthehot-rolledFe16M...

简介：TheFe-Ti-Nmateralloywaspreparedthroughthein-situreactionofnitrogengaswiththeFe-Timelt.ScanningelectronmicroscoperesultsshowthattheparticlesuniformlydistributedintheironmatrixwereTiN.ThedeliberatelypreparedFe-Ti-Nmasteralloywasemployedforthe409Lferriticstainlesssteelinanattempttorefinetheas-castsolidificationstructure.ItwasfoundthattheeffectivenessofFe-Ti-Nmasteralloyonrefiningoftheas-cast409Lferriticstainlesssteelwasaffectedbyadditionlevel,holdingtimeandmeltstemperature.Itwasfoundthattheaverageequiaxedgrainsizedecreasedfrom1503μmto303μm,theproportionofequiaxedgrainzoneincreasedfrom14%to100%withincreasingtheFe-Ti-Nmasteralloyadditionlevelto2.5%.Theproportionofequiaxedgraindecreasedfrom85%to4%asthesolidificationtemperatureincreasedfrom1803Kto1883K.Whentheholdingtimereachedto8min,thesolidificationstructuresof409Lferriticstainlesssteelshowextremepointsintheproportionofequiaxedgrain.Itisclearthatthegrainrefiningefficiencygraduallyfadeawaywiththeincreasingoftheholdingtimeattheverybeginning.However,whentheholdingtimecontinuestoincreaseandexceedstheextremepoint,thegrainrefiningefficiencyoftheFe-Ti-Nmasteralloyrecoveredtoacertaindegree.Theexperimentalresultsmentionedabovehavebeenanalyzedintermsofthermodynamics.Underappropriateconditions,theFe-Ti-Nmasteralloyusedforgrainrefinementofthesolidificationstructureof409Lferriticstainlesssteelmayhavegoodprospectsforindustrialapplications.

简介：ThemicrostructuralchangesofFe83Si4B13amorphousmotheralloyduringtheheatingprocesswereinvestigatedbyLaserScanningConfocalMicroscopy（LSCM）,andthephasetransformationwasdeterminedbytheThermo-Calccalculations.ThedifferencesinthemeltingpointsmeasuredbyDifferentialScanningCalorimetry（DSC）andLSCM,andthoseobtainedbyThermo-Calccalculationswerealsodiscussed.ItisfoundthatthemeltingpointsmeasuredbyDSCandLSCMarerelativelysimilar,whereastheonsetandendofthemeltingtemperaturescalculatedbyThermo-CalcsoftwarearehigherthanthosemeasuredbyDSCandobservedbyLSCM.

简介：Thestudyintroducesthechemicalcomposition,mechanicalproperties,physicalpropertiesandproductionprocessesoftheFe-23Mn-2Al-Vausteniticsteel.Investigationsweremadeintotheformationofcracksinthehot-rolledFe-23Mn-2Al-Vsteelplates,withopticalmicroscopy(OM),scanningelectronmicroscopy(SEM)andenergydispersivespectrum(EDS).Theresultshaveshownthatintergranularoxidationinthereheatingfurnaceisthemaincauseofthecracksonthesurfaceofthehot-rolledsteelplates.Thesurfacecrackingcanbelargelyavoidedbycontrollingtheremainingoxygencontentinthereheatingfurnaceandimprovingcontinuouscasting(CC)processestoincreasethethicknessoffineequiaxedgrainlayerofthesteelslabs.

简介：本文结合鄂钢棒材厂倍尺剪电控系统改造项目,对倍尺剪的工作原理和控制思想作简要的介绍。

简介：随着各厂开始进场采购，日本镍基不锈钢废钢价格可望在8月份全面启动。就当前而言，钢厂对于8月份发货的镍基不锈钢废钢价格并未积极砍价。

简介：采用碱熔处理样品，酸化后，移取部分溶液稀释后引入ICP测定ZrO2、TiO2、Fe2O3含量，剩余溶液用强碱分离钛、铁、锰等干扰元素后，EDTA—CuSO4法返滴定Al2O3，终点明显，检测重现性好；

简介：美国阿里根尼技术公司（ATI）扁平轧制产品单元4月10日宣布，从5月5日发货起，所有200系、300系及430合金的冷轧薄板带、精密轧制带产品，热轧、冷轧管状性质薄板带产品，明亮退火、回火薄板带和精密轧制带产品均将提高基价。该提价将通过削减两个百分点的销售折扣来实现，并将体现在经更新的冷轧不锈钢和管状性质薄板价格表中。这些价格表反映了0．0351英寸厚及更薄规格产品基价的提高。

简介：超级奥氏体不锈钢及镍基合金材料是高端装备制造业的关键材料。为推进这些材料的研发生产与推广应用，中国特钢企业协会不锈钢分会特组织召开第一届超级奥氏体不锈钢及镍基合金国际研讨会。会议主要介绍国内外石油石化、核电火电、清洁能源、船舶制造与海洋工程，以及环保等领域用超级奥氏体不锈钢和镍基合金的研发与生产、加工制造、材料选择和使用评价等情况，为国内外参会者提供交流学习的平台，吸收借鉴先进生产技术与成功应用经验，推动超级奥氏体不锈钢和镍基合金的发展。