简介:AGaP/morinnanocompositematerialwasprepared,andthekeyfactorsaffectingtheluminescentpropertiesofthematerialwereinvestigated.IntenseluminescencewasobservedafterthecompositereactionbetweenGaPnanocrystalsandmorin.TheluminescenceoftheGaP/morincompositematerialisintensifiedremarkablywiththeratioofmorintoGaPnanocrystalsincreasing,butthepeakwavelengthremainsunchanged.WiththesizeofGaPparticlesdecreasing,theluminescentintensityofthecompositeincreasesandthepeakwavelengthblue-shifts.Thepossiblereasonforthisphenomenonwasdiscussed.
简介:Widegapbrazing(WGB)experimentsusingthebuttedspecimenwitha1.5mmgapwerecarriedoutfortherepairofthefailedK418Bsuperalloylow-pressureturbinevanes.Thehightemperaturecreeprupturestrengthsofthebrazedjointsweretested,andthemicrostructuresandfracturesurfacesofthejointswereobserved.TheresultsshowthatthemicrostructureofK418Balloyjointiscomposedofdenseequiaxedgrain,smallanddiscretecompoundswithafewmicro-pores.Duringthecreeprupturetest,thecracksinitiatepreferentiallyatthemicro-poreorthegrainboundary,thenpropagatealongthegrainboundarytillthefracturehappens.Thecreeprupturestrengthat700℃ofthebrazedjointswith50%brazemetalintheworkingpartcouldexceed90%thatoftheK418Bsuperalloy,andthejointswith100%brazemetalintheworkingpartachieve70%to80%ofthecreeprupturestrengthsfortheK418Bbasemetal.