简介:随机选取青海省生产的沙棘维生素P粉样品,用原子吸收分光光度计石墨炉法测定样品中铅含量,参考《化学分析中测量不确定度的评估指南》的方法,分析铅含量测定过程中的测量不确定度的主要来源,包括溶液定容体积、称量、样品溶液铅浓度测定和测量重复性,计算合成不确定度和扩展不确定度。在该样品铅含量测定中,沙棘维生素P粉样品中铅含量为0.96mg/kg,其扩展不确定度为0.11mg/kg(置信度95%,包含因子K=2)。
简介:沙棘维生素P粉样品经微波消解处理,采用电感耦合等离子体质谱法测定样品中铁、硒、锌、钾、钠、钙、镁、铜、锰、铅、砷、汞、镉等13种微量元素的含量。使用动态反应池技术消除了多原子离子对部分被测元素的干扰。方法快速准确、灵敏度高,加标回收率在95.2%~101.8%之间,相对标准偏差小于3.0%。
简介:Inaviewofnaturalconditionsofestablishingnaturereserve,anindexsystemwaspreparedforquantitativeassessmentonstatusofendangeredspecies,andthusdegreeofendangeredspeciesinTibetwasevaluated.Takingasub-ecozoneasbasicunit,top5animalsand1plantwithhighEaswellasthenumberofspeciesineachunitwereenumerated;andthedegreeoflandutilizationwasfiguredout.Afterward,weselected6coefficients,assignedweight,andframedformulatoreckonproportionofnaturereserve,thusanareaofnaturereserveineachsub-ecozonewasobtained.In5schemesofweightassignment,aschemewithmediumareaofnaturereservewasselected.Allsub-ecozoneswereclassifiedinto4gradespriorconservation,1wasingradeA,2ingradeB,2ingradeC,and11ingradeD.Totalplannedareawasapproximately365135km2,about48834km2smallerthantheactualareaof413969km2,ratioofnaturereserveinTibetdiminishesfrom34.4%to30.38%.Basedon3factorsofhumandisturbance,ratioofbuffer-experimentalzoneinproposednaturereservewascalculated.Itwasdemonstratedthatexistingsizeofnaturereservesisexcessiveonthewhole,andtheirdistributionisnotreasonableentirely.Thesizeofnaturereservesin3sub-ecozonesofnorthernChangtangshoulddecrease,anddecrementofareaisapportionedamongother13sub-ecozoneswhichshouldincreasenaturereserve.HeterogeneityofregionaldistributionofrarespeciesinTibetisquiteobvious,soproposedareadistributionofnaturereservesismorescatteredthantheexisting.
简介:为了探讨茅台水源功能区不同林分类型的土壤养分效应,对茅台水源功能区马尾松林、柏木林和马尾松+柏木混交林3种针叶林土壤养分制征进行研究。结果表明:不同针叶林土壤平均养分存在一定的差异,其中有机质、碱解氮、速效钾质量分数均表现为柏木林〉马尾松+柏木混交林〉马尾松林,有效磷质量分数表现为马尾松+柏木混交林〉马尾松林〉柏木林,而全氮质量分数则表现为马尾松+柏木混交林〉柏木林〉马尾松林。统计分析表明:马尾松林和柏木林及马尾松+柏木混交林的有机质、碱解氮质量分数及pH值差异显著(P〈0.05),柏木林与马尾松+柏木混交林的全氮质量分数和pH值差异也显著(P〈0.05),而3种针叶林的有效磷和速效钾质量分数均不存在显著性差异(P〉0.05)。相关分析表明:全氮质量分数、有机质质量分数、碱解氮质量分数、pH值相互之间均呈显著性相关,而速效钾质量分数则与全氮、有机质、碱解氮、有效磷质量分数呈显著性相关。另外,参照土壤养分等级评价标准发现:3种针叶林的有效磷和有机质质量分数较高,均在丰富以上;速效钾质量分数则较低,均在中等以下;其他养分则在很丰富和缺乏之间。
简介:Settingmonitoringtransectinthemiddleandshallowwaterarea(altitude156-172m)inThreeGorgesreservoirhydro-fluctuationbelttoresearchthechangingcharacteristicsofthecontentsofN,P,K,pHandorganicmatterofthesoilwhichexperiencedtheinfluenceoffluctuationthefirsttime.Theresultsshowedthatbytheinfluenceofwaterlevelfluctuating,contentsofsoilN,P,K,pHandorganicmatterhadreducedindifferentsoillayersinhydro-fluctuationbelt.TheavailableNdecreasedby41.53%-59.87%,availablePdecreasedby5.26%-36.76%,availableKdecreasedby3.55%-45.56%,totalNdecreasedby9.52%-40.00%,totalPhadnochangegenerally,totalKhaddecreasedalittle,contentoforganicmaterialdecreasedby7.62%-37.83%%,pHvalueturnedtoneutral,changedby1.73%-9.58%.