简介:Differentfluxeswereusedtosynthesizelongpersistencephosphors,calciumsulfidesactivatedbyEu2+andTm3+,byconvenientsolid-statemethod.ThephosphorusingNH4Fasafluxhasgoodcrystallinityandlargeparticlesize,itsstabilityagainstwaterandotheratmosphericcomponentsisenhanced,anditsafterglowislongerandfluorescentintensityismoreintensethanthoseofthephosphorusingNH4Clasflux.TheirPLintensitiesvariedwithtimeinmoistairweremeasured,noremarkablechangewasfoundforthosepreparedwithNH4FfluxincontrastwithNH4Clasflux.SousingNH4Fasfluxisagoodmethodtoenhancethestabilityofalkalineearthsulfides.
简介:Inthiswork,boththethermalexpansionandelectricalconductivityofnanocrystallineLa2Mo2O9werestudied.ThenanocrystallinepowderofLa2Mo2O9wasobtainedbysol-gelmethod,andwiththehelpofSHP(superhighpressure)upto4.5×104atmat700℃forashorttime,andthenanocrystallinepowderwasdensifiedwithoutobviousparticlesizegrowth.TheelectricalconductivityofnanocrystallineLa2Mo2O9wasoneorderofmagnitudelowerthanthatofthemicrocrystallinesampleatthesametemperature.Owingtothephasetransition,themicrocrystallineLa2Mo2O9hasanabruptincreaseofthermalexpansionwithapeakvalueof48×10-6K-1at556℃.Forthenanocrystallinematerial,thepeakvalueincreasesto112×10-6K-1at520℃.Ontheotherhand,above600℃thesignificantgrowthofparticlesizeofthenanocrystallineLa2Mo2O9wasobserved,accompanyingbyatremendousincreaseofthermalexpansionwithapeakvalueofthirdhigherthanthatofLa2Mo2O9.
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简介:阐述了影响1Cr18Ni9Ti管坯热穿孔工艺性能的因素,剖析了不锈钢荒管产生内折和纵裂的原因,提出了防止上述缺陷的措施。
简介:文章研究了对Mg-9Gd-4Y-0.6Zr合金在时效过程中的微观组织。在225℃时效初期硬度缓慢上升,之后硬度急剧上升,24h出现了明显的时效硬化峰,然后硬度开始下降。微观结构的分析结果表明,在初期(2h)产生了大量弥散分布的具有DO19结构的β″,而在峰值时(24h)出现具有bco的β′,在持续时效(384h)时出现亚稳相β1,而在后来的长时间时效(1000h)时出现既在原位转变的平衡相β。
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简介:本文介绍了近年出现的一种技术先进、结构灵活、规模可变、价格低廉的新型集散控制系统,我们称之为中小型DCS系统或规模可变的DCS系统.并把它与传统的大型集散控制系统作了比较,希望引起大家的关注.