简介:TiO2nanometerthinfilmswithphotocatalyticantibacterialactivitywerepreparedbythesol-gelmethodonfusedquartzandsodalimeglassprecoatedwithaSiO2layer.ThethinfilmswerecharacterizedbyX-rayphotoelectronspectroscopy(XPS),scanningelectronmicroscopy(SEM),andX-raydiffraction(XRD).TheresultsshowthatsodiumandcalciumdiffusionintonascentTiO2filmiseffectivelyretardedbytheSiO2layerpre-coatedonthesodalimeglass.Theantibacterialactivityofthefilmswasdetermined.ThecrystallineofTiO2nano-meterthinfilmhasimportanteffectsontheantibacterialactivityofthefilm.
简介:Anovelantibacterialmaterial(L-PET)waspreparedbyimmobilizingε-polylysineonpolyethyleneterephthalate(PET)nonwovenfabrics.SurfacemodificationsofthefabricwereperformedbyusingachemicalmodificationprocedurewherecarboxylgroupswerepreparedonthePETsurface,acouplingagentwasgrafted,andtheε-polylysinewasimmobilized.Scanningelectronmicroscopy(SEM)wasusedtoanalyzethesurfacemorphologyofthefabrics,whilethetoluidinebluemethodandX-rayphotoelectronspectroscopy(XPS)wereusedtoevaluatethegraftingdensities.TheantibacterialactivitiesoftheL-PETwereinvestigatedbyusingtheshaking-flaskmethod.TheelectronmicrographsshowedthatthesurfaceoftheblankPETandthemodifiedfabricsdidnotchange.TheresultsofXPSanalysisconfirmedthatε-polylysinewassuccessfullygraftedontothesurfaceofPET.TheresultsoftheantibacterialexperimentsshowedthatL-PETfabricshadexcellentantibacterialactivityagainstEscherichiacoliandStaphylococcusaureus,andthatL-PETfabricswerestableinstorageforatleasttwoyears.
简介:以便区分充满的效果和暴烈的活动并且探索激发富有硅的铁矿石跟踪的活动(IOT)的方法,惰性的石英作为修正被引进标准,上好的影响,锻烧,热治好系统和一些另外的因素被红外调查,XRD,MIP,等等显微镜的方法。磨擦的试验性的结果表演和锻烧罐头仅仅改变SiO2,的非结晶的状态,IOT不在在房间温度下面治好的水泥举办暴烈的活动状况。热治好系统能刺激IOT的活动,特别压热器治好治好的臼系统能消费大量Ca(哦)2和难钙硅酸盐并且有更靠近的结构。当IOT粉末的特定的表面区域是800m2/kg,,30%水泥被IOT代替时,搽粉,有IOT的臼力量粉末比那甚至高与cementonly。
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简介:WithFe(NO3)39H2OandBi(NO3)35H2Oasrawmaterials,differentsillenite-typecompoundsandelementalbismuthwerepreparedbyafacileone-potsolvothermalmethodusingH2O,C2H5OH,(CH2OH)2andC3H8O3assolvents,respec-tively.Thestructure,morphology,elementalcompositionsandpropertiesofsampleswereexaminedbyXRD,SEM,TEM,ICP,XPS,N2adsorptionanddesorption,UV-visDRSandPL.ThephotocatalyticactivitiesofdifferentsampleswereevaluatedbythephotodegradationofRhBundervisible-lightirradiation(λ>400nm),andresultsshowthatBi36Fe2O57preparedusingC2H5OHasthesolventownstheoptimumperformance.Inordertoexplorethereactionmechanism,anadditionalexperimentwasdesignedtoinvestigatethemainactivespeciesduringthephotodegradationprocessviadissolvingdifferenttrappingagentsinthereactionsolutionbeforelightirradiation.TheresultsshowthatsuperoxideradicalanionsplayamajorroleinthissystemsincetheRhBdegradationwassignificantlysuppressedaftertheadditionofbenzoquinone.