简介:ThepreparationoftwotypesofmolecularsievesAlPO4-11andMAPO-11isreported.Theparticlesizeofthelatterishundredsofmicrons,about10timeslargerthanthatoftheformer.TheXRD,IRandDTAspectrahavedemonstratedthatmagnesiumhasbeenintroducedintotheframeworkofAlPO4-11.ThesuccessfulpreparationoflargesinglecrystalofMAPO-11willopenupanewareaforthepreparationoflargemolecularsievescrystalsinthefuture.ThelargeMAPO-11crystalcompoundisapromisinghostforthehost-guestassemblyofcompositematerials.
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简介:134Csabranchingpointins-processpathwhichisshowninFig.1.Thebranchingratioisdefinedasfβ=λβ/(λβ+λn).Itcouldbededucedfromtheabundanceof134Baand136Basince136Bagoesthroughbothdecayandneutroncaptureof134Cswhile134Baonlyexperiencesdecaychannel[1].Duetoboth134Baand134Baarepures-processnuclei,thisbranchingpointisagoodapproachtodeterminethes-processparameters.Withtemperaturedependentβ-decayrateof134Cs,thetemperatureofs-processcouldbededuced.
简介:InstitutionofModernPhysics(IMP)hasdesigned,fabricatedandinstalledthefirstSRFcavityelectropolishingsystemofChina.It’ssizedfor1.3GHzSRFcavities,andalsocanworksformultiplecellcavitieswithfurtherupgradeofstructure.
简介:Anewfuellingmethod,thesupersonicmolecularbeaminjection(SMBI)systemhasbeenappliedtoW7-ASinMay2001,supportedbytheNationalNatureScienceFoundationofChinaandtheMax-PlanckInstituteofPlasmaPhysics,Garching,Germany.TheexperimentswithhydrogenordeuteriumonW7-ASwereimplementedfortwoyears.
简介:HierarchicalZSM-11microsphereswithintercrystallinemesoporouspropertiesandrod-likecrystalsintergrowthmorphologyhavebeensynthesizedusingaspotoftetrabutylammoniumasasingletemplate.XRD,FTIR,SEM,TEMandN2adsorptionanalysisrevealedthateachindividualparticlewascomposedofnanosizedrodcrystalsinsertingeachotherandtheintercrystallinevoidsexistingamongrodsgaveasignificantmesoporesizedistribution.Steamtreatmentresultdemonstratedtheexcellenthydrothermalstabilityofsamples.Variouscrystallizationmodesincludingconstanttemperaturecrystallization(one-stagecrystallization)andtwo-stagetemperature-varyingcrystallizationwithdifferent1ststagedurationswereinvestigated.TheresultssuggestedthatthecrystallizationmodesweremainlyresponsiblefortheadjustableparticlesizeandtexturalpropertiesofsampleswhilethesmallamountoftetrabutylammoniumbromidewasmainlyusedtodirecttheformationofbothZSM-11frameworkanditsintergrowthmorphology.Furthermore,theperformanceofoptimalZSM-11asanactivecomponentforthecatalyticpyrolysisofheavyoilwasalsoinvestigated.Comparedwiththecommercialpyrolysiscatalyst,thehierarchicalZSM-11catalystexhibitedahighselectivitytodesiredproducts(LPG+gasoline+diesel),aswellasamuchlowerdrygasandcokeyield,plusahighselectivityandyieldoflightolefins(C=3C=4)andverypoorselectivitytobenzene.Therefore,fullyopenmicropore-mesoporeconnectivitywouldmakesuchhierarchicallyporousZSM-11zeolitesveryattractiveforapplicationsincleanpetrochemicalcatalysisfield.
简介:6,9,11-Trihydroxy-6a,12a-dehydrorotenoid1(coccineoneB)wassynthesizedfrom2-hydroxybenzaldehyde2andphloroglucinol.