简介：FractionsofplasmaproteinofmaleKunmingmice(bodyweight24.2±0.3g)，treatedwithCisplatini.p.injectionindoseof10mg/kg,wereobtainedbyseparationonSephadex-G-50columns,bufferedwithammoniumacetatetopH5.7,TheXSRFexperimentswereperformedattheBEPC(BeijingElectronPositronCollider)synchrotronradiationfacility.Theelements(Pt,S,Ca,Fe,Ni,Cu,Zn,Se,BrandSr)inthefractionoftheplasmaproteins(>22KD)wereassayedusinghighlysensitiveSXRF.TherelativeconcentrationsofelementswerecalculatedbyanormalizationofCOmptonscatteringintensityaround22KeV,afterthenormalizationforcollectingtimeofX-rayspectrumandthecountingoftheionchamber,andsubractingthecontributionofthepolycarbonatefilmusedforsupportingthesamples.ThedeterminationcouldprovethattheelementPtinplasmawasboundwithmacro-molecularprotein.CuandSwerepresentinthefractionoftheproteininmicetreatedwithCisplatinandexhibitedanincrease,therationoftreated/controlwere1.66±0.06and1.78±0.33repectively,whereasZndecreasedtoaratioof0.78±0.09,OurresultsareinagreementwithotherswhichshowedthatCisplatinexposureleadstoamarkedlossofkidneycopper,andamoderateriseindidneyzinc.However,thisworkmainlyfocussedontheimplementationofthisanalyticalprocedure,butnotontheresultsoftheinvestigationsoftheeffectofCisplatinontraceelementsinplasmaprotein.

简介：Copper-dopedZnOnanoparticlesweresynthesizedbythesol-gelmethod.TheX-raydiffraction(XRD)resultshowsthatZn1-xCuxO(x≤0.04)samplesaresinglephasewithZnO-likewurtzitestructure,whilethesecondaryphaseCuisobservedinaZn0.95Cu0.05Osample.MagneticmeasurementsindicatethatZn1-xCuxO(x≤0.04)samplesareferromagneticatroomtemperature.Astronggreenpeak(520nm)wasobservedexceptforUVbandpeakinphotoluminescent(PL)spectrumofZn0.98Cu0.02O.

简介：教主的联盟者组织了ZSM-5独块巨石通过转变宏的骨骼被准备多孔的硅石胶化进由帮助蒸气的conversionmethod.The形态学和宏的整体的形状的ZSM-5多孔的硅石胶化preserved.Thehierarchically很好被组织ZSM-5独块巨石展出了层次孔，与在宏内存在的中央毛孔andmacropores多孔的硅石胶化，并且ZSM-5.Theproducts形成的微毛孔被使用XRD，SEM和N_2adsorption-desorptionmethods适当地描绘了。

简介：HighorderBraggscattering(M=2andM=3)operationsofthedistributedfeedbackdyedopedsol-gelsilicalasersareachievedusingthesecondharmonicoutputofaNd:YAGlaserasthepump.Laserlinewidthoflessthan0.06nmandconversionefficiencyof0.7%forM=3and11%forM=2aremeasured.Wavelengthtuningofabout15nmaroundtheemissioncenterhasbeenrealizedbyvaryingtheintersectionangle.

简介：有一致的杆形状的单斜晶的LaPO4nanostructures被一个简单大音阶的第五音胶化方法成功地综合了。过程包含形成同类，透明，metal-citrate-EDTA胶化先锋，由锻烧列在后面支持胶化先锋的热分解产出LaPO4nanoparticles。他们的形态学和结构被XRD，TEM，TG-DSC和HRTEM描绘。结果显示单个单斜晶的阶段LaPO4nanorods乐意地在800点被获得吗？在3h以内。而且，做Eu3+的LaPO4nanocrystals的光致发光(PL)描述被执行。在PL性质上做内容的锻烧温度和Eu3+的效果详细被详细描述。房间温度光致发光(PL)描述表明光亮度以及到5D0-7F2的5D0-7F1的紧张比率高度依赖于锻烧温度，并且Eu0.05La0.95PO4nanophosphor与最强烈的排放显示出相对有希望的PL表演。

简介：

简介：为尖晶石铁酸盐nanomaterial合成的大音阶的第五音胶化汽车燃烧方法的最近的开发和趋势简短被讨论并且极其分析了。能被用于合成过程的更好的理解和微观结构的控制和尖晶石铁酸盐nanopowder产品的性质的反应的各种各样的参数的分析是这篇评论文章的主要目的。特殊注意对粒子尺寸和阶段纯净的变化被给予。为这些目的在complexant，氧平衡和燃烧过程化学药品添加剂，以及加热机制和空气之间的关联，被建立。这些结果从申请的立场是相关的并且铁酸盐处理。

简介：Inthispaper,anovelSPMEmode,PDMS-coatedsolidglassmicrospheres(SGMs),werepreparedbysol-gelmethod.UsinghomemadethermaldesorptionunitcoupledwithCGC-FID,sixPAHsasmodelanalytes,theperformanceofthenewmodewascharacterized.Thenewextractivephaseexhibitedhighthermalstabilityandsatisfactoryextractioncapability.Thedetectionlimitswere0.01-0.045ng/mL,andthelinearitywasfrom0.5ng/mLto96ng/mL.TheR.S.D.sofrepeatabilityforretentiontimeandpeakareawereallwithin0.074%and6.7%,respectively.TherecoveriesofthePAl-Iswere78-127%fromthesamplestakenfromriverwater.

简介：Nanocrystallineoxidedispersionstrengthened(ODS)ferriticsteelpowderswithnominalcompositionofFe-14Cr-3W-0.3Ti-0.4Y2O3aresynthesizedusingsol-gelmethodandhy-drogenreduction.AtlowreductiontemperaturetheimpurityphaseofCrOisdetected.AthigherreductiontemperaturetheimpurityphaseisCr2O3whicheventuallydisappearswithincreasingreductiontime.ApureODSferriticsteelphaseisobtainedafterreducingthesol-gelresultantproductsat1200℃for3h.TheHRTEMandEDSmappingindicatethattheY2O3particleswithasizeofabout15nmarehomogenouslydispersedinthealloymatrix.ThebulkODSferriticsteelsamplespreparedfromsuchpowdersexhibitgoodmechanicalperformancewithanultimatetensilestressof960MPa.

简介：

简介：Modifiedsensingmembranesbasedonfluorescencequenchingwerepreparedbythesol-gelmeth-od,usingformamideasthedryingcontrolchemicaladditive,tetraethoxysilaneasthemainmaterial,Ru(phen)3Cl2astheindicator.Themembranewiththeoptimumthicknessof20-50μmisuniformandcrack-free,inwhichtheindicatorhasaverysmallleakingrate.Themembraneisimmersedinwaterfor50h,themembranesensingparameterMdecreasesbylessthan5%.Thefiberopticoxygensensorwiththesensingmembranehasadetectionlimitof5×10-6M(ppm),aresponsetimeoflessthan30s,excellentreproducibilityandstability.

简介：PHProteomicDB是一个写PHP的模块在proteomics帮助研究人员用个人网络站点分享二维的电气泳动胶化数据。不技术或除了一些基础，PHP知识是必要的。PHProteomicDB让一个用户友好的政府连接进入并且更新数据。即时地显示胶化特征，胶化图画，和数的胶化点，他们的相关鉴定在蛋白质数据库指向他们的参考页创造网页。模块在http://www.huvec.com/index.php3是自由地可得到的?rub=Download。

简介：

简介：Threenewcatalystsbasedonthesilicagelsupportedpolyetherionicliquids(ILs),i.e.,[HO-PECH-MIM]Cl-Si,[H2N-PECH-MIM]Cl-Si,and[HOOC-PECH-MIM]Cl-Si,wereprepared,andtheirchemicalstructureswerecharacterizedbyinfrared(IR)spectroscopyandnuclearmagneticresonance(NMR)spectroscopy.Thermogravimetricanalyzer(TG),X-raydiffractometer(XRD)andscanningelectronmicroscope(SEM)wereusedtoevaluatetheirthermalstability,crystallinestructureandapparentmorphology,respectively.SurfaceareasofthepreparedcatalystswerecalculatedbytheBrunauer-Emmett-Teller(BET)method.Thecatalyticreactionforthesynthesisofpropylenecarbonate(PC)usingCO2andpropyleneoxide(PO)inthepresenceofthepreparedcatalystswasstudied.Theinfluencesoftimesofrecyclingandcatalyststructureoncatalyticperformancewerealsoinvestigated.TheexperimentalresultsshowedthatthesilicagelsupportedpolyetherILscatalystssuccessfullypreparedundermildconditioncouldpossesstheadvantagesofhighactivity,excellentthermalstability,goodselectivityandeasyrecycling,whilethephasetransitionoftheliquidpolyetherILscatalystswasalsoachieved.Whenthereactiontemperaturewas90°C,theCO2pressurewas2.0MPaandthedosageofthecatalystwas2.5%,[HOOC-PECH-MIM]Cl-Siwasfoundtohavethebestcatalyticperformanceinthecatalyticprocess,withtheconversionratereaching100%andtheselectivityequatingto98.2%.Theconversionrateandselectivitystillcouldreachmorethan90%evenafterthecatalystwasreusedfor15times.

简介：

简介：ThisPaperreportsenrichmentandsepqrationoftracePd(Ⅱ）withsilicagelbondedby(benzolyazo-arsenazoI)-aminopropyl(BAAI·SG).BAAI·SGisstableinsolutionbetween6mol/LHClandpH9.0.ThemaximumadsorptivecapacitiesofBAAI·SGandSGare52.7,23.5μmol/grespectively.AfterpreconcentrationthroughBAII·SGcolumn,Pd(Ⅱ）ofppblevelinartificialwatersamplescanbemeasuredbyspectrophotometry.

简介：Magneto-opticFaradayrotationeffectandtheamountofbismuthsubstitutedinyttriumirongarnetsinglecrystalfilmspreparedbygel-coatingonmodifiedgadolinium-galliumgarnetsubstratesareinvestigated,wherethegelissynthesizedbyasol-gelreactionofnitratesandethyleneglycol.Thecoatedgelisannealedinairattemperaturesupto660℃for4h,whichisabout300℃lowerthanthatofliquid-phaseepitaxy.ThemaximumamountofBisubstitutionisx=2.7andthecrystallizationtemperatureofgarnetphasedecreaseswiththeincreaseofxdownto520℃forx=2.7.Inthisfilm,ahugeFaradayrotationof-8.1×104(°)/cmatλ=0.633μmisobtained.

简介：Asystematicstudyonthesynthesisandantibacterialactivityofthequaternary"onium"saltsgraftedonaninsoluble"gel-type"stryene-7%divinylbenzenecopolymerbypolymer-analogousreactionsisshowed.Antibacterialactivityofquaternaryammoniumand/orphosphoniumsaltsgraftedonpolymer-supportshasbeenstudiedagainststaphylococcusaureusandEscherichiacoli.Awidevarietyof"onium"saltsboundtomacromolecularsupportswithdifferentquaternarygroupsanddifferentquaternarychainlengthsubstituentswereexamined.Theantibacterialactivityofmixed"onium"saltsincreasesasaconsequenceoftheassociationofammoniumandphosphoniumsaltsgraftedonthesamepolymericsupport.

简介：4-hydroxy-4'-nitroazobenzene(NHA)and4-amino-4'-nitroazobenzene(DO3)werepreparedrespectivelyfromp-nitrophenylamineasaprecursorcompound.Twokindsofdopedorganic/inorganichybridnonlinearoptical(NLO)materialscontainingNHAandDO3weresynthesizedbySol-Gelprocess.ThepreparationandpropertiesoftwoNLOmaterialswerestudiedandcharacterizedbyFTIR,1H-NMR,UV-VIS,SEM,DSCandSHGmeasurements.TheresultsshowthatthemaximumdopingamountsofNHAandDO3intwodopedhybridNLOmaterialsare7.2(wt)%and11.3(wt)%respectively,andthecorrespondingsecond-orderNLOcoefficients(d33values)are2.91×10-8esuand6.14×10-8esu.TwodopedNLOmaterialshaverelativelygoodRTstability,after90daysatRTthed33valuescanmaintainabout85%oftheirinitialvalues,butafter10hat100℃canonlymaintainabout50%oftheirinitialvalues.Inthisreport,thereasonsforhigh-temperatureinstabilityofdopedmaterialswerediscussed,andthepossibleimprovementswerealsosuggested.

简介：narG基因经常为细菌的减少硝酸盐的社区分析被用作一个分子的标记。在这研究，指向narG基因的教材的一个新集合被设计并且把使中毒反应的坡度胶化电气泳动(PCR-DGGE)试金用于嵌套半的聚合酶链。新教材的潜力在直接从在中央、南部的意大利散布的五个不同试验性的地点从土壤提取的DNA上被验证。教材的特性被切除决定，扩大，并且乐队定序由DGGE解决了。种系发生的分析显示出在从学习的土壤检索的序列和narG序列之间的关联从并且-Proteobacteria。这些教材扩展了存在为在土壤的减少硝酸盐的细菌的社区的尺寸和差异上的生态的学习的分子的工具。