简介:Wehaveobservedsomekindsofdefectsinunseededrapidzone-melting-recrystallized(RZMR)SifilmsformedwithaRF-inducedgraphitestripheatersystem,usingcross-sectionspecimenelectronmicroscope.Theobserveddefectsaresubgrainboundaries(SGB),dislocationsandmicrotwins.ThemostcommonlyobserveddefectsareSGBwhichformedasaresultofsomeorientationdifferencesbetweenadjacentgrainsduringtheirrapidself-nucleationgrowth.MixedtypeSGBwerefrequentlyobserved,althoughsomepuretiltortwistSGBexistedalsointheSifilms.Therotationangularcomponentaroundtheaxisparalleltoscanningdirectionismuchlargerthanthataroundotheraxes.SGBconsistprimarilyofarraysofdislocationandhavecrystallographicangulardeviationsofonedegreeorless.DuringSifilmcooling,dislocationsandmicrotwinswereformedduetonon-uniformthermalstress.ThecrystallographiccharactersofthedislocationsinSifilmsarethesameasthoseincommonbulkSisinglecrystals.TheirBurgersvectorsareb=a/2<110>.Somedis-locationsrunacrosstheSifilm,andtheamorphousSiO2layersonandunderneaththeSifilmcaneffectivelyblockthedislocationsandpreventthemfromenteringthelayers.MicrotwinswereobservedintheSifilmssometimes,thetwinningplanesbeing{111}.