简介：Thecreationandpropagationoflongitudinalacousticphonons(LAPs)inhighqualityhematitethinfilms(α-Fe2O3)epitaxiallygrownondifferentsubstrates(BaTiO3,SrTiO3,andLaAlO3)areinvestigatedusingthefemtosecondpump–probetechnique.Transientreflectionmeasurements(?R/R)indicatethephoto-excitedelectrondynamics,andtheinitialdecaylessthan1psandtheslowdecayof～500psareattributedtotheelectron-LOphononcouplingandelectron–holenonradiativerecombination,respectively.LAPsinα-Fe2O3filmcanbecreatedbyultrafastexcitationoftheligandfieldstate,suchastheligandfieldtransitionsunder800-nmexcitationaswellastheligandtometalcharge-transferwith400-nmexcitation.Thestrainmodulationsofthesoundvelocityandtheout-of-planeelasticpropertiesaredemonstratedinα-Fe2O3filmondifferentsubstrates.

简介：在G-度量空间中,获得了非线性压缩算子F:X×X→X满足混合-g-单调性质下的耦合叠合点结果.减弱了压缩条件,所得结果也是近期文献相关结果的推广.

简介：本文用三种方式给出计算队长L(t)的瞬时分布。

简介：对于广义G—M模型，如果最小二乘估计（LSE）与最佳线性无偏估计（BLUE）相等，就可以用LSE代替BLUE反之，用LSE代替BLUE就要蒙受一些损失．有时，这种损失可能是很大的，因而研究这种损失的大小就显得颇为重要．本文提出了一种新的相对效率，并给出了该相对效率的上下界，最后讨论了该相对效率与广义相关系数的关系．

简介：在这份报纸，我们在公制的Lp(R)(1p)得到平均-B宽度和Sobolev班Brp(R)的无限的维的-G宽度的准确价值并且获得准确(N)和强壮的asymptotic(>1)在公制的Lq的Sobolev牛肉熏香肠班Wrpq(R)的无限的维的-G宽度的结果在公制的Lqp(R)(1qp)的(R)和它的双盒子Wrp(R)。

简介：本文在半序度量空间中引进了g-可比较算子和耦合不动点和9-不动点这些新概念,研究了9-可比较算子的g-耦合不动点或g-不动点存在性问题,得到了几个存在性定理.所得结论推广了最近一些文献中的主要结果.

简介：利用2种杂化的密度泛函DFT方法（BHLYP和B3LYP）,2种纯DFT方法（BLYP和BP86）,以DZP＋＋为基函数对Cl2O5/Cl2O5-的平衡构型进行了量子化学计算,研究了它们的几何构型、相对能量和振动频率,并对Cl2O5/Cl2O5-体系的电子亲和势进行了理论预测.

简介：3,5,6,8-Tetrahydro-4H-thiopyrano[4′,3′:4,5]thieno[2,3-d]pyrimidin-4-ones(7)weresynthesizedviathebasecatalyticreactionsofaminesorphenolswithcarbodiimides(5),whichwereobtainedfromtheaza-Wittigreactionsofiminophosphoranes(4)witharomaticisocyanates.

简介：提出fuzzy映象序列的公共fuzzy混合不动点的概念，研究了g-非扩张型fuzzy映象序列的公共fuzzy混合不动点定理，我们所得的定理改进和推广了近期相关的重要结果。

简介：Immobilizedtriazinedyeaffinitychromatographyhasbeenwidelyusedforproteinpurification.Inthispaper,CibacronBlueF3G-4wasimmobilized,throughaspacerarm,ontoarigidhydroplhilicporouspolymerbyreactinganepoxy-group-containingpoly(vinylalcohol)with6-aminohexyl-N'-CibacronBlueF3G-A,whichwasobtainedbyreactingCibacronBlueF3G-4withexcessof1,6-diaminohexane,inapH8.6buffer,Theepoxy-group-containingpoly(vinylalcohol)waspreparedbytreatingmacroporouspoly(vinylalcohol)withexcessepichlorohydrininthepresenceofNaOHindimethylsulfoxide.Themacroporouspoly(vinylalcohol)waspreparedbyhydrolysisofmacroporouscrosslinkedpoly(vinylacetate),whichwassynthesizedbysuspensioncopolymerizationofvinylacetateandtriallylisocyanurateinthepresenceofbutylacetateandn-heptaneasdiluents.TheCibacronBlueF3G-A-immobilizedpoly(vinylalcohol)waspackedinastainlesssteelcolumn(250×5mmI.D.)andthechromatographicbehaviorsofseveralproteins(cytochromec,lysozyme,bovineserumalbumin,insulin,andlactatedehydrogenase)weredetermined.

简介：针对指数分布2／3（G）表决系统产品，本文给出了系统的寿命分布及数字特征，并在全样本场合下给出了参数的矩估计、极大似然估计和逆矩估计，通过大量Monte—Carlo模拟比较了三种点估计的精度。此外。还给出了求参数区间估计的两种方法，并通过大量Monte—Carlo模拟考察了区间估计的精度，得到参数的精确区间估计优于近似区间估计。

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简介：一个图称为分数（g，f，m）一消去图若删除任意m条边后的剩余子图依然存在分数（g，f）一因子．本文证明若图G的阶为n，1≤n≤g（x）≤f（x）-△≤b-△对任意顶点x∈V（G）成立，δ（G）≥（b-△）（b＋1）/a＋2m,n≥（a＋b）（2（a＋b）＋2m-1）/a＋△且｜NG（x1）∪NG（x2）｜≥（b-△）n/a＋b对任意不相邻顶点x1和x2都成立，则G是分数（g，f，m）-消去图．这个领域并条件在一定程度上是最好的．

简介：Inthispaper,westudytheexistenceanduniquenessofsolutionstostochasticdifferentialequationsdrivenbyG-Brownianmotion(GSDEs)withintegral-Lipschitzcoefficients.

简介：ThemolecularsieveVPI-5wassynthesizedbyusingvariousorganicamines(DEA,Di-PA,DBA,DPenA,TBA,DEOAandTEOA)asthestructure-directingagent.TheuseofDPAenlargedtherangeofthecrystallizationtemperaturefrom110℃to190℃inthesynthesisofVPI-5,whiletheuseofTEOAchangedthecompositionofthereactantsinabroadvariety.DiaminesarethetypicalaminesinthesynthesisofVPI-5.AmongthemDBAandDPAarethemostfavoritestructure-directingagentsforthesynthesisofVPI-5molecularsieve.

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简介：通过DSC和同步辐射WAXS技术测定了结晶温度对iPP和TMB-5/iPP结晶行为的影响.结果表明,随等温结晶温度升高,iPP总结晶度变化不大,但是β晶型含量降低的同时α晶型含量增加.TMB-5是一种具有温度依赖的选择性成核剂,当等温结晶温度高于140℃时,含TMB-5成核剂的iPP的β晶型的含量急剧降低.本文进一步探讨了TMB-5对iPP结晶行为影响的机理.

简介：Aseriesof5-aminolevulinicacidanditsalkylestermethanesulfonateswasexploitedtophotodynamictherapy(PDT)ofhumanlymphocyticcells,U-937invitro.ThePDTefficiencyisinfluencedbytheconcentrationandincubationtime.Generally,forALAanditsalkylestermethanesulfonates,thecellsurvivalratedecreasesandtheaccumulationabilityofPpIXincreaseswiththeconcentrationandincubationtime.Wefoundthatthelongercarbonchainmethanesulfonates(C5-S,C6-S,C8-S)exhibitbetterPDTeffectthanALAmethanesulfonate.ThispossiblyprovidesapromisingroutetotheclinicalapplicationofPpIX-mediatedPDTtocancercell.

简介：4,4-Dialkyl-2-oxazolin-5-onesarepreparedbyonestepreactionof2-oxazolin-5-onewiththemagnesiummethylcarbonate(MMC)andalkyIhalides.Itisanovelandconvenientmethodforsynthesisofα,Υ-disubstitutcdα-aminoacidbyhydrolysisof4,4-dialkyl-2-oxazolin-5-ones.

简介：TheexternalsurfaceofHZSM-5zeolitewaspassivatedbyliquidsiliceousdepositionandbyacidicsitespoisoningwithlepidine,respectively.Thenmethanol-to-hydrocarbons(MTH)reactionwasinvestigatedovertheaboveas-preparedcatalystsandthedissolublecokeontheseusedcatalystswasanalyzedbyGC-MS,tostudytheroleoftheexternalsurfaceofHZSM-5inthecatalyticreaction.ComparisonwiththeexperimentalresultsbasedonparentZSM-5showedthattheproductdistributionofMTHreactionwasobviouslyinfluencedbytheexternalsurface.Evidenceswerelistedasfollows:(1)thefinalproductonparentHZSM-5showedhigheraromaticselectivity,lowerolefinselectivity,lowerratioofC2/C3+aliphaticsandhigherratioofC3/C4+aliphaticsthanthereactionmixtureproducedbythesolecatalysisofacidicsitesinHZSM-5channel;(2)alittleofpentamethylbenzeneandhexamethylbenzeneintheproductonparentHZSM-5,wasproducedviamulti-methylationofmethylbenzeneontheexternalsurface.TheaboveconclusionmayalsobesuitableforMTHreactionoverotherzeoliteswith10-ringchannel.