简介：ThreenovelC2-symmetricmacrocyclescontainingpyridylunitshavebeenpreparedbythecycliccondensationofchiraldiamideintermediateswith2,6-pyridinedicarbonyldichlorideinhighlydilutedsolutionatroomtemperature.

简介：本文利用四元数矩阵的广义Frobenius范数建立一个关于四元数矩阵的实函数，并讨论了它的极值问题．然后在四元数矩阵方程AX-YB=C的解集合中导出了与给定矩阵的最佳逼近解的表达式．

简介：研究了线性空间C[a，b]上的线性相关性，给出了衡量C[a，b]上n个函数线性相关性程度的量以及线性相关的充分必要条件．

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简介：PtRu/SnO2/Ccatalystwaspreparedinapolyolprocess,followedbyreductiontreatmentandalkalineetching.X-raydiffraction,transmissionelectronmicroscopewithenergydispersivespectrometerandXrayphotoelectronspectroscopywereusedtocharacterizethemorphology,structureandcompositionofthecatalysts.COandmethanolelectro-oxidationactivitiesofthecatalystswereevaluatedbyCOstrippingvoltammetry,cyclicvoltammetryandchronoamperometrymeasurements.ReductiontreatmentofthepreparedPtRuSnO2/CcatalystinapolyolprocessinducedtheenrichmentofSnonthesurface,inhibitingmethanoldissolutionandCOadsorptiononPt.AlkalineetchingremovedSnorSnOxandthusexposedPtRuonthesurface,resultinginenhancedactivitiesforCOandmethanolelectro-oxidationduetothesynergyeffectsofPtRuonthesurfaceandSnspeciesbeneath.

简介：基于不确定语言变量和区间模糊数，提出了不确定区间隶属度语言变量的概念，定义了不确定区间隶属度语言变量的运算规则、大小比较方法，给出了不确定区间隶属度语言变量的加权算术平均算子、加权几何平均算子及其相应性质，并将这些算子应用于属性权重确知且属性值以不确定区间隶属度语言变量形式给出的不确定多属性群决策问题中，通过示例验证了基于不确定区间隶属度语言变量信息的多属性群决策方法的有效性和可行性。

简介：Arylhalidesareakindofextremelyvaluablecompoundsusedintransition-metal-catalyzedcouplingreactions,aswellasimportantstructuremotifsinmanynaturalproductsandmanufactureddrugs[1,2].Theclassicalapproachforpreparationofhaloarenesiselectrophilicaromaticsubstitution(EAS)usingvarioushalogenatingreagentsoroxidativehalogenationswithhalogenatingreagentgeneratedinsitufromhalidesandoxidants,suchasperoxide,oxygenandmeta-cholorperoxybenzoicacid(mCPBA)[3,4].However,harshreactionconditionsarerequiredforhalogenationoflessactivearomatics.orthoMetalationfollowedbyhalogenquenchingisanotherapproachforhalogenationofaromatics[5].However,thereareobviousdrawbacksforthesemethods,suchaslowregioselectivity,harshconditionsandevendangerousprocedures.Therefore,thedevelopmentofanalternativeandpracticalwayremainschallengeinorganicsynthesis.

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简介：IntroductionFritillariahupehensisHsiaoetK.C.HsiaisaliliaceousplantgrowinginthesouthwestdistrictofHubeiProvince,China.ItsbulbshavebeenrecordedinthePharmacopoeiaofthePeople′sRepublicofChinaasoneoftheprincipaltraditionalChineseherbsnamed"Hubeibeimu"[1].

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简介：设T（t）是Lq（1＜q＜∞）空间上的C0-半群，A为其无穷小生成元．本文证明若T（t）是弱LP稳定的，则其生成元的谱界是负的。由LotzWeis最近得到的关于Lq（Ω）空间中正C0半群的增长界等于生成元的谱界这一结果得出，Lq（Ω）空间中正C0半群弱Lp稳定与指数稳定等价．

简介：主要讨论了自反Banach空间中一类C0-半群族{h（t）}稳定性问题，证明了此类半群族{Th（t）}指数稳定与L^p-稳定是等价的．

简介：研究二次矩阵方程X2-bX-C=O（b〉0,C为n×n阶正定阵）的正定解,证明了解的存在唯一性并且给出了求解方法.

简介：<正>Inthispaper.basedonlargedeviationformulasestablishedinstrongertopologygeneratedbyH(?)ldernorm,weobtainthefunctionallimittheoremsforC-Rincrementsofk-dimensionalBrownianmotioninH(?)ldernorm

简介：Tris)(η5-cyclopentadienyl-μ-carbonyl-iron)-μ3-nitrosylclusterwasobtainedfromthereactionofcyclopentadienyldicarbonylirondimerwithnitrogenmonoxideinxylene.Theclusterwascharacterizedbyelementalanalyses,IR,MSand1HNMR.Thecrystalstructureof[(η5-C5H5)(μ-CO)Fe]3(μ3-NO).C4H8OwasdeterminedbyX-raydiffractionanalysis.ItcrystallizesintheorthorhombicspacegroupPnma,a=9.053(2),6=10.545(2),c=22.525(4)A,V=2150.3(7)A3,Z=4,Dc=1.68g.cm-3;structuresolutionandrefinementbasedon1141reflectionswithI>3.0(I)(MoKa,A=0.71073A)convergedatR=0.0540.Theinfraredabsorptionbandat1325cm-1oftheμ3-NOinthecluster,whichisredshifted,showsthatμ3-NOisactivated.

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简介：Toeffectivelysolvetheagglomerationproblemsinthesolidstatereactionprocess,pre-addingglucoseisadoptedtothesynthesisofLiFePO4/CenergymaterialsusingFe–Pwasteslag.Theaverageparticle&grainsizeofLiFePO4/Cdecreases,andtheimpuritiesinLiFePO4/Ccompositesreducetoagreatextent.Itmakesgreatsensetothemassindustrialproduction.Theoptimumsynthesisconditionsdeterminedinthisworkarebasedontheorthogonalexperiments.Thesamplessynthesizedinascaleof500gexhibithighpurity,excellentelectrochemicalperformance,highreactionactivity,goodreversibility,andlowpolarizationlevel.Thedischargecapacitiesare145,134,117,and102mAh/gatthecurrentdensitiesof0.1C,0.2C,0.5Cand1C,respectively.ThisworkputsforwardapracticalsuggestionformassproducingenvironmentalbenignandlowcostLiFePO4/Cascathodematerialsoflithiumionbatteries.

简介：证明了(C-K)性质,(S-K)性质,L-KR空间,L-KS空间和CL-KR空间和CL-KS空间的一些充要条件.这些条件表明了(C-K)与(S-K)性质,L-KR与L-KS空间及CL-KR空间与CL-KS空间之间的对偶性质.

简介：给出了C^n单位球上的Bloch空间上的复合算子的下有界的一个充分条件和一个必要条件。对必要条件得出了较优的结论．

简介：通过在谐振腔内插入窄带滤光片,开展了XeF（C-A）蓝绿激光窄线宽输出实验研究。研究结果表明,采用该方法,可以获得焦耳量级能量、线宽小于2nm、波长稳定的激光输出,激光最窄线宽为1.3nm。增大滤光片与谐振腔光轴的入射角,激光器输出能量降低。