Layereddoublehydroxides(LDHs)areaclassoflayeredinorganicmaterialsthatconsistofstructurallypositivelychargedlayersandexchange-ableanionsintheinterlayergalleryforchargebal-ance.ThedelaminationofLDHsisdecidedbysyn-thesismethodtosomeextent.Inthiswork,LDHsaresynthesizedviathreedifferentroutesandtheirdelaminationpropertiesarecharacterized.Co-precipitationmethodion-exchangemeth-