简介：Whenmeasuringresidualstressofcoarse-grainaluminumalloyusingX-raydiffractionmethod,thediffractionprofileshowstwopeaksandpositionofmeasured2dwillbechanged,whichleadtoaninaccuratemeasurementresult.Hence,inthispaper,somemethodswereemployedtoimprovethemeasurementaccuracy.Duringthemeasuringprocess,differentparameters(diameterofirradiatedarea,Ψ-oscillationrangeandexposuretime)wereselectedandprofilepeakshiftmethodwasutilized.Moreover,whenthe20ofprofileswasdetermined,differentcalculationmethodswereusedtocalculatetheresidualstress.TheresultsshowthatdiameterofirradiatedareaandΨ-oscillationrangehavesignificantinfluenceonthemeasuringresult.Forstressvaluecalculateddirectlyfromthetestequipment,crosscorrelationmethodismoreaccuratethantheabsolutepeak.Furthermore,anothertwocalculationmethodsofslopewith2θ-sin~2Ψande-sin~2Ψwereusedtocalculatethestressbasedonparameters(2θ,ε)obtainedfromcrosscorrelationmethod.Itisconcludedthat20-sin~2Ψmethodcanfurtherimprovethemeasurementaccuracy.

简介：本文采用真空钎焊工艺对1Cr18Ni9Ti不锈钢进行了焊接,焊后通过扫描电镜、电子探针扫描、XRD等分析测试手段对试样进行分析研究。研究结果表明:试样表面生成了碳化物,为TiC和Ti8C5;表面碳化物的生成过程是在真空高温环境下,Ti元素与环管中向外扩散的C发生固相扩散反应生成TiC,过量的Ti再与TiC反应生成Ti8C5。