简介:Thioglycolicacid(TGA)-stabilizedCdTenanocrystals(NCs)werepreparedwithsodiumtelluriteastelluriumsource,whichavoidsthecumbersomeprocessesassociatedwithH2TeorNaHTesources.FluorescentCdTe/SiO2compositesweresynthesizedbyasol-gelmethodwithouttheexchangeofsurfaceligands.ThephasestructureofCdTeNCswasinvestigatedbyX-raydiffractometry.Forcomparison,somecharacterizationsweredoneforboththeCdTeNCsandthecomposites.CdTeNCsandCdTe/SiO2compositeswerecharacterizedwithTEM,digitalcameraandfluorescencespectrophotometer.ThestabilityofCdTeNCsandthecompositeswereinvestigatedinphosphate-bufferedsaline(PBS)bufferandthefluorescentpropertiesofthecompositeswerediscussedindetail.
简介:Inthisarticle,nano-scaleAl/Fe2O3compositeswithdifferentmorphologiesweresuccessfullyobtainedbyasimpleelectrospinningtechnique,whichisbasedonasurfactant(polyvinylpyridine,PVP)inamixtureofN,N-dimethylformamide(DMF)and2-propanol.TheelectrospunAl/Fe2O3compositesexhibitedacrystalstructureandphasecompositionbyX-raydiffractionanalysis.ThedifferentmorphologiesoftheAl/Fe2O3compositeswerealsoobservedthroughscanningelectronmicroscopyandtransmissionelectronmicroscopy.Itwasfoundthattherathersimpleelectrospinningmethodusedtopreparethemorphology-controlledAl/Fe2O3compositesmayhavethepotentialforpreparationofpropellants,explosives,andpyrotechnicsinthefuture.