简介：Thesolutionreactionmechanisms,composition,donoratoms,propertiesofcoordinatelinkandstabilityofthecomplexesonthesystemsofadrenalinewithNa3+,Gd3+andTm3+havebeenstudiedbypH-potentiometrictitrationandelectronicspectroscopy.Adrenalineperturbsthef-felectronictransitionofNd3+andTm3+sothattheabsorptionspectraoftheircomplexesareshiftedtowardlongerwavelengths.Theabsorptionspectraofthecomplexesformedbythethreef-blockelementionswithadrenalineareshiftedtowardshorterwavelengthswiththeincreaseofPHinΔγ=350～650nm

简介：YbAl3(BO3)4crystalofgoodopticalqualitywasgrownbythefluxmethod.ThestructureofYbAl3(BO3)4crystalwasdeterminedbysingle-crystalX-raydiffraction.TheexperimentshowsthatYbAl3(BO3)4belongstothedoubleborateswithatrigonalstructure.ThespacegroupisR32anditsunitcellconstantsweremeasuredtobea=0.92965nm,c=0.72129nm,V=0.53673nm3,Z=3.Thetransmittancespectraweremeasured.Thecut-offofYbAl3(BO3)4crystalis216nm,andtherearetwoabsorptionpeakslocatedat940and975nmfrom190nmto2600nm.ThethermalpropertiesofYbAl3(BO3)4crystalwerestudiedforthefirsttime.Theaveragethermalexpansioncoefficientsweredeterminedtobe2×10-6/℃,9.5×10-6/℃alonga-andc-direction.ThespecificheatofYbAl3(BO3)4crystalwasmeasuredtobe0.6695J·(g·℃)-1atroomtemperature.AllresultsindicatethattheYbAl3(BO3)4crystalisanexcellentstoichioimetriclasermaterial.

简介：本文采用高温团相反应合成TCaTiO3∶Pr3+红色发光材料、报道了Pr3+激活的CaTiO3的光谱特征及长余辉特性，并与CaS∶Eu的光谱特性及长余辉进行了比较。CaTiO3∶Pr3+将是一种具有广泛用途的新材料

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简介：在石灰窑大修过程中对石灰窑存在的薄弱环节采取了一些改进措施，建造新型石灰窑可以从根本上扭转公司石灰生产的被动局面。

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简介：针对原燃料条件恶化,制定出各项合理的操作制度,使3#高炉各项技术指标大为改善,特别是节焦效果明显。

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简介：Redphosphor(Y,Gd)BO3:Eu3+withgrainshape,smallsize,non-agglomerate,highcrystallinityandgoodphotoluminescence(PL)intensitywaspreparedbyacomplexmethodthattheprecursorofthephosphorwaspreparedbyco-precipitationmethodandthephosphorwaspreparedbycombustionmethod.TheSEMphotosandthephotoluminescencespectrumexcitedunderVUVshowthatthemorphologyandluminescentpropertiesofthisphosphoraresatisfiedwhenanappropriateamountofureawasadoptedasthecombustionagentinthepreparationprocedure.

简介：TheelectrodeprocessofY3+iononmolybdenumandnickelelectrodeshasbeenstudiedbycyclicvoltammetryandchronopotentiometryintheYCl3-NaCl-KClmelt.Theoverallchargetransferprocessisatwo-stepreaction:Y3++e=Y2+;Y2++2e=Y.YttriumreducedonthenickelelectrodecanformaseriesofNi-Yalloys.X-raydiffractionanalysiswasemployedtodeterminethealloycompositionsformedunderdifferentcon-ditions.

简介：3#高炉实行强化冶炼，各项技术经济指标都有长足的进步，但强化必须有精料作前提，各项新技术的应用相辅相成。不断完善操作制度。

简介：ThephotocatalystsK4Nb6017andK4Nb6017dopedwithFe^3+andCr^3+werepreparedbysolidstatereactionandwerecharacterizedbypowderx-raydiffraction,UV-visdiffusivereflectanceandscanningelectronmicroscopy.ThephotocatalyticactivityofK4Nb6O17andK4Nb6O17dopedwithFe^3+,Cr^3+wereinvestigatedwithmethanolaselectrondonorandPtaspromotercatalystunder+400nmUVirradiation.Thedifferenceofphotocatalyticactivitybetweenthemwasalsodiscussed.TheindividualrateofhydrogenevolutionfortheK4Nb6O17,Fe-K4Nb6O17andCr-K4Nb6O17asphotocatalystsare5.35,5.00,6.25mmol·L^-1.h^-1respectively.

简介：TheZrO2-Al2O3ceramiccompositeswerepreparedbyappropriatetechniqueswithcommercialZrO2andAl2O3powdersasrawmaterialsandY2O3asstabilizer.TheresultsindicatethatwiththeintroductionofAl2O3intotheZrO2matrixwherethequantityofadditiveY2O3is3.5%(molefraction),thegrowthofZrO2grainsisefficientlyinhibited,whichhelpstheZrO2grainsexistinametastabletetragonalmanner;thushigherstrengthandtoughnessareacquired.Whenthecontentofaluminais20%(massfraction),thebendingstrengthandfracturetoughnessofthecompositesare676.7MPaand10MPa·m1/2respectively,themechanicalbehaviorsareclosetothosepreparedwithZrO2andAl2O3powderssynthesizedthroughwetchemicalapproach.Themechanicalbehaviorsofthecompositesarewellimprovedowingtothedispersiontougheningofaluminagrainsandphasetransformationtougheningofzirconiagrains.

简介：Ternarycomplexesofeuropiumandterbiumwithbenzoicacidand1,10-phenanthroline[RE(BA)3phen](BA=benzoatephen=1,10-phenanthroline)wereintroducedintoasilicamatrixbysol-gelmethod.Thethermalstabilityandluminescencebehaviorofthecomplexesinsilicagelswerestudiedincomparisonwiththecorrespondingsolid-statecomplexesbythermaldecomposition,excitationandemissionspectra.Thethermalstabilityofthecomplexesisenhancedinsilicagelmatrixandtheluminescenceremainesunchanged.

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简介：3#高炉1999年2月投产,2005年4月降料线停炉中修,5月15日点火开炉,达产时间快,6月份即取得较好经济技术指标。

简介：ＡｐｐｌｉｃａｔｉｏｎｏｆｔｈｅＥｕ３＋ＩｏｎｆｏｒＳｉｔｅＳｙｍｍｅｔｒｙＤｅｔｅｒｍｉｎａｔｉｏｎＢｉｎｎｅｍａｎｓＫ，Ｇｏｒｌｌｅｒ－ＷａｌｒａｎｄＣ(ＵｎｉｖｅｒｓｉｔｙｏｆＬｅｕｖｅｎ，ＤｅｐａｒｔｍｅｎｔｏｆＣｈｅｍｉｓｔｒｙ，Ｃｏ?..

简介：TheLa3+-loadedadsorbentwaspreparedbythereactionbetweenLa3+andethanolamine-modifiedvegetabletannicextract,totreatF--containingwastewater.TheproblemsofheavycolorcausedbyvegetabletannicextractandofturbiditycausedbyreactionbetweenLa3+andF-weresolved.Whenotherconditionswerenotchanged,pH,temperature,stirringtime,anddosewerechangedrespectivelyandtheadsorbancewastestedrespectively.Theresultsshowthatthisadsorbentpossesseshighsaturatedadsorptivecapacity(18.86mg·g-1)whenpHis5～6,T≤80℃,0.2gdosage,and180minagitatingtime,andtheadsorbancereachesthehighest(98.5%).Theadsorbentcanbeeasilyregeneratedwith0.5mol·L-1NaOHatpH12.