简介：

简介：

简介：AnimprovedmethodhasbeendevelopedforenrichinganddeterminingtraceIn,Pt,Sn,Co,Hg,Pb,Ni,Bi,Pd,CuandAginhigh-puritygallium.SamplewastreatedbyPDM（partialdissolutionofmatrix）withHCl（11mol/L）-HNO3（0.5mol/L）toasmallresidueofwhichGawasthenremovedbyextractionwith1mlisopropylether.TheconcentratedimpuritiesweredeterminedbyAESprocedure.Therecoveriesfortheele-mentsattherangeof0.02～0.2μgare95～103％;therelativestandarddeviationsfordeterminedimpuritiesoverarangeofn.10-7～n·10-8％are4.3～12％;thedetectionlimitofmostelementscanreachn·10-7～n·10-8％levelwiththeexceptionofHgandPt.Thismethodhasbeensuccessfullyusedtoanalyzemanysam-plessentbyfactoriesandinstitutes.

简介：Inlasernon-penetrationdeeppenetrationweldingprocess,weldingmaterialwillvaporize,metalvaporandambientgaswillproduceahigherdegreeionization,whichformsplasmaofhighconcentration.Inthecaseofformingasmallhole,plasmawillejectfromthehole,andformacousticemission(AE)signals.BecauseAEinformationhasmanyadvantagessuchasnon-contactmeasuring,fastresponse,andhighratioofsignaltonoise,itcanbeusedasamonitorvariableforin-processcontrol.BystudyingAEinformation,informationofweldingpoolandsmallholecanbeobtained.AccordingtocharacteristicofAEinformation,thispaperrevealsthecorrelationbetweenweldingparametersandAEsignals,andprovidesagoodbaseforfurtherqualitycontrol.