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97 个结果
  • 简介:Thepreliminarydesignofamulti-barrelspelletinjectorwithcyclerefrigeratorasanadvancedplasma-fuellingtoolforHL-2Atokamakhasbeenproposed.Thedesignaimsatprecisetemperaturecontrol,easyoperation.withhighreliabilityandhighflexibility.GM-cyclerefrigeratorandpipe-gunStructurehavebeenemployedtoproduce25pelletsin25gunbarrelssimultaneouslyandthedesignaims.havebeenaccomplished.Primedesignprinciple,engineeringparameters,structureandlayoutofthecryostatcomponentsaswellascalculationofheatloadforthecryostatarepresented.

  • 标签: 托卡马克装置 球形注射器 循环制冷 热量损失 散热片
  • 简介:TheprecisionofplasmaelectrondensityandFaradayrotationanglemeasurementisakeyindicatorforfar-infraredlaserinterferometer/polarimeterplasmadiagnosis.Toimprovetheprecision,anewmulti-channelhighsignal-to-noiseratioHCOOHinterferometer/polarimeterhasbeendevelopedontheHL-2Atokamak.Ithasahigherlevelrequirementforphasedemodulationprecision.Thispaperintroducesanimprovedreal-timefastFouriertransformalgorithmbasedonthefieldprogrammablegatearray,whichsignificantlyimprovestheprecision.Wealsoapplyareal-timeerrormonitoringmodule(REMM)andastableerrorinhibitingmodule(SEIM)forprecisioncontroltodealwiththeweaksignal.Wetesttheinterferometer/polarimetersystemwiththisimprovedprecisioncontrolmethodinplasmadischargeexperimentsandsimulationexperiments.Theexperimentalresultsconfirmthattheplasmaelectrondensityprecisionisbetterthan1/3600fringeandtheFaradayrotationanglemeasurementprecisionisbetterthan1/900fringe,whilethetemporalresolutionis80ns.ThisperformancecanfullymeettherequirementsofHL-2A.

  • 标签: HL-2A装置 等离子体诊断 电子密度 转角测量 控制处理 高精度
  • 简介:InHL-2Atokamaks,thebehaviorofheatfluxdepositedonthedivertortargetshasbeenstudiedduringdeuteriumgasfuelling.Theheatfluxisreducedsignificantlyaftersupersonicmolecularbeaminjection(SMBI)fuellingduringOhmicandelectroncyclotronresonanceheating(ECRH)divertordischarges.TheSMBIfuellingcausesanincreaseintheplasmadensityandthischangeresultsintheexperiencedchangeoftheedgeproperties.MostofthisreductionindivertortargetheatfluxoccurstogetherwithahighplasmaradiationregionlocatedatneartheX-point.Thelargestreductioninheatfluxprofilesisobservedattheoutboarddivertorseparatrixstrikepoint,whiletheheatfluxfarfromthestrikepointremainsalmostunchanged.Inparticular,withSMBImulti-pulsesgasfuelling,apartiallydetacheddivertorregimeisobservedwithahighlyradiatingregionattheX-point.Withtheonsetofthepartiallydetacheddivertorregime,asuddendropinbothheatfluxandpowerflowonthedivertortargetisobserved.Thereductioninpowerloadonthedivertortargetsisroughlyequaltotheincreaseinplasmaradiationloss.

  • 标签: 偏滤器靶板 HL-2A装置 热通量 红外热像 HL-2A托卡马克 等离子体密度
  • 简介:Theγ-Fe2O3nanoparticlescoatedwithDBSandCTABwerepreparedbythemicroemulsionmethod.Thecoatedsamplesshowenhancednonlinearopticalpropertiescomparedwiththeirbulkcouterpart.The.Moessbauerspectraatroomtemperatureweremeasuredforthecoatedferricoxides.Themonolayersoftheorganicmoleculearefoundtohaveastrongchemicalbondwiththesurfaceatomsandthushaveasignificantinfluenceontheelectronstructureofparticlesurface.@1999ActaMetallurgicaInc.

  • 标签: 氧化铁 纳米粒子结构 表面活化剂 DBS CTAB
  • 简介:TheNi-AlalloycontainingCr,FeadditiveswerepreparedasRaneyNiCatalystbyhighenergymilling.ThesizeandsurfacestateofNi-Alalloypowderwerestudiedbyparticlesizeanalyzerandsanningelectronmicroscopy.theStructurewasanalyzedbyXRDandMoessbauermethods.Theresultsshowedthatafterahigh-energymilling(HEM).theNi-Alalloytransformstoanano-scaleNiAlstructurewithrichAl.Byannealingthealloy,ametastableNi2Al3phasecanbeobtained.

  • 标签: 催化剂 催化剂镍 纳米晶体
  • 简介:ThetransientopticalpropertiesofnovelPbSnanoparticlescoatedwith2.6-O-diallyl-β-cyclodextrines(CDs)werestudiedbythefemtosecondpump-probetechnique.Theresultsshowthattheultrafasttransient-inducedabsorptionforthenovelcase.ComparedtothePbSnanoparticlesstabilizedwithpolyvinylalcohol(PVA),wefindthattheprocessforthenovelcaseisdifferentfromthePbS(PVA),WesuggestthattheCDssurfacemodificationcantrapholesonthesurfaceofPbSnanoparticles.ThiscaninduceanefficientchargeseparationbetweenthePbSnanoparticlesanditssurfaceandresultinanultrsafast-inducedabsorptionfornovelPbSnanoparticles.

  • 标签: PBS 纳米颗粒 表面化学处理 非线性光学特性
  • 简介:Thenanoparticlesγ-Fe2O3coatedwithsurfactants.DBS,STandCTAB.repsectively.weresynthesizedbymicroemulsionmethod.Thecoatedferricoxides.whichshowenhancednonlinearopticalpropertiescomparedwiththeirbulkcounterpart.wereprobedbyEXAFSinsolutionforms.Thex=-rayabsorptionspectraforFeKedgeweremeasuredatroomtemperaturebyhelpofsynchrotronradiationlightsource.Extendedx-rayabsorptionfinestructureanalysisshowsthatthecoatinglayersoforganicmoleculesinteractwithsurfaceatomsofnanopartices,theFe-Obondlengthwasextended.

  • 标签: 氧化铁 纳米粒子 涂层 有机活化剂 EXAFS
  • 简介:Themicrostructuresofloadedorganicphasesofthreequaternaryaminesolventextractionsystemsforgold,whichwereN263-xylene,N263-tributylphosphate(TBP)-dodecaneandN263-2-ethylhexanol(isooctanol)-dodecane(N263-trialkylmethylammoniumchloride;alkyl=C8-C10),werestudiedbyFouriertransforminfrared(FTIR)spectroscopyandextendedX-rayabso\rptionfinestructure(EXAFS)spectroscopy.AccordingtotheEXAFSresults,itwasfoundthatthegoldcoordinationenvironmentwasthesamebeforeandafterextraction.However,theC≡NstretchingvibrationsofAu(CN)2-werealsofoundtobedifferent,InordertoexplainthedifferencesintheIRcharacteristicsofC≡Ninthethreeextractionsystems,threemicrostructuremodelsareproposed.FortheN263-xylenesystem,themodelisasimpleionpair.Fortheothertwosystemswithamodifier(TBPandisooctanol),themodelsaretwosupramolecularstructuesbasedonhydrogenbondingbetweenthemodifierandAu(CN)2^-.SomerelatedworksuchasonthehydrationofacetonitrileandthefinestructureofC≡NinsolidKAu(CN)2wasalsoperformedinordertoofferadditionalsupportingevidenceforthereliabilityoftheproposedmodels.

  • 标签: 溶剂提取 微结构研究
  • 简介:《ASME锅炉与压力容器规范》第Ⅷ卷第2册包含了压力容器及其相关的泄压装置的设计、材料、制造、检验、检查、试验、认证的强制性要求、具体禁令和非强制性指导。该文献旨在说明用于锅炉与压力容器规范第Ⅷ卷第2册的设计计算。

  • 标签: ASME 压力容器规范 手册 非强制性 设计计算 泄压装置
  • 简介:AseriesofoxideizedCO-K-Mo/γ-Al2O3catalystsamples,preparedbyimpregnatingoxidizedK-Mo/γ-Al2O3sampleswithanaqueoussolutionofcalculatedCo(NO3)2andthencalcininginairattemperaturesof350℃,500℃65℃and800℃respectively,weresulfidedandtheninvestigatedfortheactivityinthesynthesisofmixedalcoholsfromCOhydrogenationunderconditionsofp=5.0MPa,T=350℃andGHSV=4800h^-1.TheresultsdemonstratethattheadditionofcobaltpromoterisfavorabletotheformationofhigheralcoholsandtheopimumcalcinationtemperaturesafterimpregnatingwithCo^2+areabout500-650℃.ThestructureofCoandMospeciesontheoxidizedandsulfidedsampleswasdeterminedbyX-raydiffraction(XRD),laserRamanspectrum(LRS)andextendedX-rayabsorptionfinestructure(EXAFS).Foroxidizedsamplecalcinedat350℃,cobaltexistsasCo3O4spectiesandcoversthesurfaceofK-Mo-Ospecies,thestructureofK-Mo-OspeciesisthesameasthatinK-Mo/Al2O3sample.TheinteractionbetweencobaltandK-Mo-Ospeciesisrelativelyweak.Aftersulfidation.Cobaltexistsassulfidecrystalliteswithanoctahedralcoordinatedstructure,andmolybdenumasMoS2crystallites.Foroxidizedsamplescalcinedat500-650℃,CocomponentinteractswiththeK-Mo-Ospeciesanddestroysthelong-rangeorderoftheK-Mo-Ospectesgradually,Aftersulfidation.CotendstoexistasasulfidewithtetrahedralcoordinatedstructureandMostillasMoS2crystallites.Foroxidizedsamplecalcinedat800℃,CocomponentexistsmainlyasCoAl2O4species,mostofwhichcannotbesultidedduringsulfidation.

  • 标签: 催化剂 催化活力 混合醇合成
  • 简介:ToobtainthermotolerantmutantsofG.oxydans,whichcanenhancethetransformationrateofL-sorboseto2-Keto-L-gulonate(2-KLG)at33℃inatwo-stepprocessofvitaminCmanufacture,ionbeamwasusedasamutationsource.GluconobacteroxydansGOandBacillusmegateriumB0wereusedinthisstudy.TheoriginalstrainGluconobacteroxydansGOwasmutatedbytheheavyionimplantationfacilityattheInstituteofPlasmaPhysics,ChineseAcademyofSciences.SeveralmutantsincludingGluconobacteroxydansGI13wereisolatedandcoculturedwithBacillusmegateriumB0at33℃inshakingflasks.TheaveragetransformationrateofthenewmixedstrainGI13-B0inpergram-moleculereached94.4%aftersevenpassagesinshakingflasks,whichwasincreasedby7%whencomparedwiththeoriginalmixedstrainG0-B0(GluconobacteroxydansG0andBacillusmegateriumB0).Moreover,thetransformationrateofI13B0wasstableat94%attemperaturesrangingfrom25℃to33℃,whichwouldbeofmuchvalueinreducingenergyconsumptioninthemanufactureofL-ascorbicacid,especiallyintheseasonofsummer.Toclarifysomemechanismofthemutation,thespecificactivitiesofL-sorbosedehydrogenaseinbothG0andGI13wereestimated.

  • 标签: 山梨糖 转化率 耐热突变体 离子束 等离子物理