SYNTHESIS AND CATALYTIC HYDROSILYLATION PROPERTY OF POLYSILOXANE-SUPPORTED MERCAPTOSELENAETHER PLATINUM OR RHODIUM COMPLEX-中国期刊网

摘要 Silica-boundmercaptoselenaether-containingsilsesquioxaneanditsplat-inumorrhodiumcomplexweresynthesizedfromγ-(2,3-epithiopropyl)propyltrimethoxysi-laneviaring-openingreactionwithbis(2-hydroxyethyl)sclenide,followedbyhydrolysisandimmobilizationonfumedsilica,andthenreactingwithpotassiumchloroplatiniteorrhodiumchlorideinacetoneundernitrogenatmosphere.Itwasfoundthattwonoblemetalcomplexescancatalyzethehydrosilylationofolefinswithtriethoxysilaneeffectively.Theinfluencesoftemperature,theamountofcomplexused,thenatureofolefinoncatalyticactivitywereinvestigated.

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SYNTHESIS AND CATALYTIC HYDROSILYLATION PROPERTY OF POLYSILOXANE-SUPPORTED MERCAPTOSELENAETHER PLATINUM OR RHODIUM COMPLEX

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SYNTHESIS AND CATALYTIC HYDROSILYLATION PROPERTY OF POLYSILOXANE-SUPPORTED MERCAPTOSELENAETHER PLATINUM OR RHODIUM COMPLEX

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