Microstructure evolution of an Ni-Cr-Co base superalloy heat-treated at 704 and 760℃

(整期优先)网络出版时间:2003-03-13
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Thermodynamiccalculation,SEM(scanningelectronmicroscopy),TEM(transmissionelectronmicroscopy),XRD(X-raydiffraction),phaseextraction,andchemicalanalysiswereemployedtostudythephasestabilityandphaseprecipitationinanewNi-Cr-Cobasesuperalloyheat-treatedat704and760℃foralongtime.Theresultsshowthattheprecipitatesofthisnewalloyheat-treatedatstandardannealingconditionandheat-treatedat704and760℃foratimeupto2000hareγ′,MC,M23C6,andM6C,andηphaseformsatgrainboundariesandinmatrixofsamplesheat-treatedat760℃aswell.Themassfractionsofγ′(+η),MC,M23C6,andM6Cinallsampleshavenolargechangeswithanincreaseinagingtime,butγ′precipitatesgrowobviously.Theγ′-to-ηtransformationinthesamplesheat-treatedat760℃tookplacewithincreasingagingtime.TheηprecipitatesformaWidmanstattenpattemandtheγ′phaseshaveremeltedpartlyinthesamplesheat-treatedat760℃.Thealloymaintainsabettermicrostructuralstabilityduringprolongedagingat704℃,butaworsemicrostructuralstabilityduringprolongedagingat760℃.