简介:Toeffectivelysolvetheagglomerationproblemsinthesolidstatereactionprocess,pre-addingglucoseisadoptedtothesynthesisofLiFePO4/CenergymaterialsusingFe–Pwasteslag.Theaverageparticle&grainsizeofLiFePO4/Cdecreases,andtheimpuritiesinLiFePO4/Ccompositesreducetoagreatextent.Itmakesgreatsensetothemassindustrialproduction.Theoptimumsynthesisconditionsdeterminedinthisworkarebasedontheorthogonalexperiments.Thesamplessynthesizedinascaleof500gexhibithighpurity,excellentelectrochemicalperformance,highreactionactivity,goodreversibility,andlowpolarizationlevel.Thedischargecapacitiesare145,134,117,and102mAh/gatthecurrentdensitiesof0.1C,0.2C,0.5Cand1C,respectively.ThisworkputsforwardapracticalsuggestionformassproducingenvironmentalbenignandlowcostLiFePO4/Cascathodematerialsoflithiumionbatteries.
简介:ThinheavilyMg-dopedInGaNandGaNcompoundcontactlayerisusedtoformNi/AuOhmiccontacttop-GaN.ThegrowthconditionsofthecompoundcontactlayeranditseffectontheperformanceofNi/AuOhmiccontacttop-GaNareinvestigated.Itisconfirmedthatthespecificcontactresistivitycanbelowerednearlytwoordersbyoptimizingthegrowthconditionsofcompoundcontactlayer.WhentheflowrateratiobetweenMgandGagassourcesofp++-InGaNlayeris10.6%andthethicknessofp++-InGaNlayeris3nm,thelowestspecificcontactresistivityof3.98×10-5?·cm2isachieved.Inaddition,theexperimentalresultsindicatethatthespecificcontactresistivitycanbefurtherloweredto1.07×10-7?·cm2byoptimizingthealloyingannealingtemperatureto520℃.
简介:Inthispaper,weintroduceaconditionweakerthantheLpdifferentiability,whichwecallCpcondition.Weprovethatifafunctionsatisfiesthisconditionatapoint,thenthereexiststhebestlocalapproximationatthatpoint.WealsogiveanecessaryandsufficientconditionforthatafunctionbeLpdifferentiable.Inaddition,westudytheconvexityofthesetofclusterpointsofthenetofbestappoximationsoff,{Pe(f)}ase→0.
简介:Inthispaper,wesolvethequadraticp-functionalinequalities‖f(x+y)+f(x-y)-2f(x)-2f(y)‖≤‖ρ(2f((x+y)/2)+2f((x-y)/2)-f(x)-f(y))‖,(0.1)whereρisafixedcomplexnumberwith|ρ|<1,and‖2f((x+y)/2)+2f((x-y)/2)-f(x)-f(y)‖≤‖ρ(f(x+y)+f(x-y)-2f(x)-2f(y))‖,(0.2)whereρisafixedcomplexnumberwith|ρ|<1/2.Usingthedirectmethod,weprovetheHyers-Ulamstabilityofthequadraticρ-functionalinequalities(0.1)and(0.2)incomplexBanachspacesandprovetheHyers-Ulamstabilityofquadraticρ-functionalequationsassociatedwiththequadraticρ-functionalinequalities(0.1)and(0.2)incomplexBanachspaces.
简介:AKerr-lens,mode-lockedYVO4∕Nd:YVO4lasercoupledwithanacousto-opticmodulator(AOM)Q-switchingnear1064nmwasemployedtopumpanintracavityKTiOPO4(KTP)opticalparametricoscillator.Asubnanosecondsignalwavenear1572nmwithlowrepetitionratewasrealized.AtanAOMrepetitionrateof8kHz,themaximumoutputpowerwas165mW.Thehighestaveragepulseenergy,theshortestduration,andthehighestpeakpowerofamode-lockingsignalpulsewereestimatedtobe~10.3μJ,~120ps,and~82kW,respectively.
简介:Li4Ti5O12(LTO)/carbonnanotubes(CNTs)compositematerialissynthesizedbasedonasolid-statemethodbysand-milling,spray-dryingandcalciningat8508CunderN2flow.TheLTO/CNTssampleswith1wt%and3wt%weightratioofCNTsadditionandthepristineLTOsampleareprepared.TherateperformanceandthethermalstabilityofthesesamplesareinvestigatedbasedonLiMn2O4(LMO)/LTOfull-cell.TheresultsshowthattheweightratioofCNTsadditionhasdistincteffectonLTOperformances.ThecompositematerialsofLTOcompositedCNTshavebetterperformanceathigh-rateduetotheintercalationenhancementbyconductivenetworkofCNTs.Atsecond,theoverchargingtemperatureresponseofthecell’ssurfacewith1wt%CNTsadditionisthelowest.Theparticlesizedistributionismeasuredandthemostuniformparticlesareobtainedwith1wt%CNTsaddition.ThistrendcouldexplainthatthemediumquantityofCNTsisoptimaltoimprovetheheatandmasstransferandpreventtheproblemsofcrystallitegrowinginterferenceandaggregationduringthecalcinationprocess.
简介:LetL=L0+VbethehigherorderSchrdigertypeoperatorwhereL0isahomogeneousellipticoperatoroforder2mindivergenceformwithboundedcoefficientsandVisarealmeasurablefunctionasmultiplicationoperator(e.g.,including(-?)m+V(m∈N)asspecialexamples).Inthispaper,assumethatVsatisfiesastronglysubcriticalformconditionassociatedwithL0,theauthorsattempttoestablishatheoryofHardyspaceHpL(Rn)(0<p≤1)associatedwiththehigherorderSchrdingertypeoperatorL.Specifically,wefirstdefinethemolecularHardyspaceHpL(Rn)bytheso-called(p,q,ε,M)moleculeassociatedtoLandthenestablishitscharacterizationsbytheareaintegraldefinedbytheheatsemigroupe-tL.
简介:4-(Succinimido)-1-butanesulfonicacidasanefficientandreusableBronstedacidcatalyzedthesynthesisofpyrano[4,3-b]pyranderivativesundersolvent-freeconditions.Thecatalystcanbepreparedbymixingsuccinimideand1,4-butanesultonethatismoresimpleandsaferthanthepreparationofsuccinimidesulfonicacid.Thismethodhastheadvantagesofhighyield,cleanreaction,simplemethodologyandshortreactiontime.Thecatalystcouldberecycledwithoutsignificantlossofactivity.