简介：对金银花中Mn,Fe,Cu,Zn,Ca和Mg6种金属元素的化学形态进行了分析。用传统的煎煮法把元素提取以后,分别采用0.45μm微孔滤膜、LSA-10大孔吸附树脂柱、正辛醇/水分配体系,以区分元素的可溶态和悬浮态、有机态和无机态、醇溶态和水溶态,最后用火焰原子吸收光谱法（FAAS）对湿法消解以后的各种元素进行测定。结果表明,6种元素的提取率在14.97%～48.54%,悬浮态的颗粒吸附率在4.02%～19.84%,加标回收率在96.58%～103.9%,RSD（n=6）≤2.4%。

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简介：ThechoicenumberofagraphG,denotedbyX1(G),istheminimumnumberksuchthatifalistofkcolorsisgiventoeachvertexofG,thereisavertexcoloringofGwhereeachvertexreceivesacolorfromitsownlistnomatterwhatthelistsare.Inthispaper,itisshowedthatX1(G)≤3foreachplanegraphofgirthnotlessthan4whichcontainsno6-,7-and9-cycles.

简介：AseriesofdoubleperovskitesRSrMnFeO_6(R=La,Pr,Nd,Sm)wassynthesizedundermildhydrothermalconditions.Crystalgrowthsofthesamplesweresensitivetoalkalinity,temperature,fillingfraction,andcompositionofinitialreactionmixture.ThedesiredseriesofcompoundsbelongstotheclassofAA'BB'O_6perovskiteswitharandomdistributionofMnandFeatomsovertheB-cationsub-lattice.TheirstructuresshowthedistortedorthorhombicsymmetrywithspacegroupPnma.TheshapesandsizesofthecrystalswereanalyzedonaRigakuJSM-6700Fbyscanningelectronmicroscopy.AnalysisdonebyXPS,MssbauerspectroscopyandiodometrictitrationrevealsthatMnandFeionshave+4and+3oxidationstates,respectively.

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简介：Onenewsesquiterpenecompound,namely,illihenlactoneA（1）,andonenewprenylatedC6–C3compound,illihenryioneH（2）,alongwiththreeknownsesquiterpenes（3–5）wereisolatedfromthestemsofIlliciumhenryi.Thestructuresof1and2wereelucidatedbyspectroscopicevidenceincludingNMR,HRESIMSandcirculardichroism（CD）.Compound2exhibitedaweakinhibitoryratioforbglucuronidasereleaseinducedbyplatelet-activatingfactor（PAF）inratpolymorphonuclearleukocytes（PMNs）invitro.

简介：Ti6Al4Visawidelyappliedinmedicalimplantssuchasbone,joint,andteethduetoitsexcellentmechanicalproperties,corrosionresistance,plasticityandthebiocompatibilityofthesurfaceoxide.However,thenativesurfaceoxidefilmisquitethin(about5nm)andtechniquessuchasmicroarcoxidation,plasmasprayedhydroxyapatitaeandplasmaimmersionionimplantationareusedtosynthesizethickersurfacetitaniumoxide.

简介：TheCADSdemofacilityisaimedtobuildaprototypelinacforthelowenergypartofthecontinuouswave(CW)superconductingprotonlinacanddemonstratetechnologyinthissection[1].IntheCADSroadmap,therealizationof25MeV10mAbeamisakeypoint.Thus,basedonthe10MeVCADSInjectorIIatIMP,IMPandIHEPwillbothcontributeacryomoduletoreach25MeVatthesiteofIMP[2].Todumpthebeamfromthelinac,webuildanewhighenergybeamtransportlinewithbendingangleof90°,toavoidback-scatteringgammaandneutronbeamstodamagethelinac.Fig.1showsthelayoutofthe25MeVdemofacility.

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简介：用量子化学原理,CIS/6-31＋G（d,p）方法研究了2-甲基环戊酮离子前6个激发态的解离过程,通过虚频的振动分析,计算其可能产物,寻求2-甲基环戊酮离子的解离通道和解离产物.

简介：Inthiswork,SMAT(surfacemechanicalattritiontreatment)wasperformedonTi6Al4V.PlasmanitridingoftheSMATedsampleswasinvestigatedincomparisonwithcoarse-grainedsamples.Thesampleswerecharacterizedusingopticmicroscope,SEM,TEMandVickersmicrohardnesstester.TheresultsshowedthatasignificantlythickercompoundlayerwithhigherhardnesswasobtainedfortheSMATedsampleswhencomparedwithun-SMATedsamplesafternitriding.CorrosionresistanceofTi6Al4VinaRinger’ssolutionwasstudiedbyelectrochemicaltechniquesincludingopencircuitpotentialmeasurement,potentiodynamicpolarizationandEIS(electrochemicalimpedancespectroscopy).Overall,ourresultsidentifiedthebeneficialimpactsoftheduplexSMAT/nitridingtreatmentoncorrosionbehaviourofTi6Al4V.Weartestswerealsoperformedonaball-on-disctribometerwherethetreatedsampleswererubbedagainsta6mmdiameteraluminaballunderanormalloadof5NusingRinger’ssolutionaslubricantmedia.ThefrictioncoefficientoftheSMATedandnitridedsampleswasreducedcomparedtotheuntreatedsamples.WearratesdemonstratedthatSMATcombinedwithnitridingimprovedwearresistanceofTi6Al4Valloy.

简介：Segmentedblockcopolymerbasedonnylon6(N6)andpolyethyleneoxide(PEO)withstochiometricratiowassynthesizedviaatwo-stepprocess.ThefirststeprepresentsendcappingofN6inthepresenceofadipicacidleadingtocarboxyterminatedN6,andthesecondoneispolycondensationofthelatterproductwithPEOinthepresenceofcatalystandthermostabilizertoformahighmolecularweightmulti-blockcopolymer.SeveralmethodswereappliedtocharacterizethesynthesizedcopolymersuchasFouriertransforminfraredspectroscopy,protonnuclearmagneticresonancespectroscopy,differentialthermalanalysis,differentialscanningcalorimetry,X-raydiffractionandatomicforcemicroscopy.Theobtainedresultsconfirmedthemulti-blockstructureforcopolymerwithaveryhighdegreeofmicro-phaseseparation.Atomicforcemicroscopymicrographsindicatedthatthemorphologywasthedispersionofhighstiffnessnanostructuredpolyamide(PA)domainsintheamorphousregionofPEOmatrix,whichcanbeveryimportantintheirperformanceformembraneprocesses.

简介：<正>近几年来海南省关于轴对称、平移与旋转这方面的中考试题,常见的题型有选择题、填空题、网格作图题,主要考查的内容为轴对称、平移与旋转的基本性质.但在2014年的中考命题中,网格作图已不在是主要的考查方式,而是将旋转的有关内容与其它的几何内容相结合,变成一道综合性有点强的填空题,从而达

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简介：Inanattempttofindnewantitumoragents,anovelclassofchromonecompoundswithabenzimidazoleorabenzoxazoleringinpositions2or6weresynthesizedviacondensationinpolyphosphoricacid(PPA)byusingchromoneacidsasthestartingmaterials.Duringthepreparationprocess,itwasfoundthatPPAcouldcleavethechromoneringtoproducearing-openingcompound(6).Themolarratioofthechromonecompound(5)tothering-openingcompound(6)variedwiththechangeofreactiontemperatureandtime.BasedonMTTprotocol,theantitumoractivityofeachofthecompoundsobtainedwasevaluatedagainstthreehumancancercelllines:KB(oralepidermal),A2780(ovary)andBel7402(liver).TheIC50variedfrom54.7μmol/Ltomorethan180μmol/L.

简介：证明了图2Kv的可旋转(4,6)圈系存在的充分必要条件为:v≥10,v≡0,5(mod10).更多还原

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