学科分类
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500 个结果
  • 简介:采用2步水热法合成了LaPO4∶Eu3+-Fe3O4复合材料.在LaPO4∶Eu3+-Fe3O4复合材料中,LaPO4∶Eu3+为单斜晶相,呈纳米棒状,纳米棒直径和长度分别为20-100nm和0.2-1μm;Fe3O4为正交晶相、呈20-30nm颗粒状,Fe3O4粒子紧紧附着在LaPO4∶Eu3+纳米棒表面;样品磁性和发光性质研究表明所合成LaPO4∶Eu3+—Fe3O4复合材料既具有发光性质又具有磁性.

  • 标签: LaPO4∶Eu3+-Fe3O4 水热 发光 磁性
  • 简介:路易斯底能从CF3SiMe3和包含羰基混合物催化-trifluoromethyl酒精形成。-trifluoromethyl白酒能也被用来处于基本条件支持合成,这被发现。

  • 标签: 有机合成 有机化学 催化反应
  • 简介:X-rayimagingistheconventionalmethodfordiagnosingtheorthopedicconditionofapatient.ComputerizedTomography(CT)scanningisanotherdiagnosticmethodthatprovidespatient’s3Danatomicalinformation.However,bothmethodshavelimitationswhendiagnosingthewholeleg;X-rayimagingdoesnotprovide3Dinformation,andnormalCTscanningcannotbeperformedwithastandingposture.Obtaining3Ddataregardingthewholeleginastandingpostureisclinicallyimportantbecauseitenables3Danalysisintheweightbearingcondition.Basedontheseclinicalneeds,ahardware-basedbi-planeX-rayimagingsystemhasbeendeveloped;itusestwoorthogonalX-rayimages.However,suchmethodshavenotbeenmadeavailableingeneralclinicsbecauseofthehightcost.Therefore,weproposedawidelyadaptivemethodfor2DX-rayimageand3DCTscandata.Bythismethod,itispossibletothreedimensionallyanalyzethewholeleginstandingposture.TheoptimalpositionthatgeneratesthemostsimilarimageisthecapturedX-rayimage.Thealgorithmverifiesthesimilarityusingtheperformanceoftheproposedmethodbysimulation-basedexperiments.Then,weanalyzedtheinternal-externalrotationangleofthefemurusingrealpatientdata.Approximately10.55degreesofinternalrotationswerefoundrelativetothedefinedanterior-posteriordirection.Inthispaper,wepresentausefulregistrationmethodusingtheconventionalX-rayimageand3DCTscandatatoanalyzethewholelegintheweight-bearingcondition.

  • 标签: 2D-3D REGISTRATION 3D analysis X-RAY CT
  • 简介:Synthesisofinorganicnanostructureswithspecificsizeandwelldefinedmorphologieshasattractedconsiderableattentionduetotheirsuperiorelectrical,optical,magnetic,andchemical

  • 标签: 纳米结构 FE2O3 合成 笼状 自由 三维
  • 简介:BSTOdielectricceramicwaspreparedfromSrTiO3andBaTiO3powderssynthesizedbyhydrothermalmethod,aswellasfromBa0.6Sr0.4TiO3powdersynthesizedbyconventionalsolid-statereaction.Theformercanbesinteredatarelativelylowtemperatureof1120℃.CharacterizationbySEMshowedthatthegrainshapesofbothceramicsarecubical,thoughthegrainsizeoftheformerismuchsmaller.Dielectricconstantsmeasuredat20℃wereshowntovarywithfrequencyintherangefrom1kHzto2MHzanddcbiasfield,andfurtherthatthedielectriclossoftheformertobelessthan2×10-3inthefrequencyrangeof20kHzto1MHz,muchsmallerthanthatofthelattersample.Fortheformer,temperaturedependenceofdielectricconstantismuchflatterandthereexistsanextendedphasetransitiondiffusioncoveringawidetemperaturerangeofCurietemperatureTc.Thesmallergrainsizeoftheformerdepressesthedcbiaselectricalfielddependenceofdielectricconstant.Thetunabilityis7%underabiasfieldof0.6kV/mmdc.

  • 标签: 钛酸锶钡陶瓷 钛酸钡粉体 介电性能 水热合成 介电常数测量 高频
  • 简介:Temperature-dependentphotoluminescencecharacteristicsoforganic-inorganichalideperovskiteCH3NH3PbI3-xClxfilmspreparedusingatwo-stepmethodonZnO/FTOsubstrateswereinvestigated.Surfacemorphologyandabsorptioncharacteristicsofthefilmswerealsostudied.Scanningelectronmicroscopyrevealedlargecrystalsandsubstratecoverage.Theorthorhombic-to-tetragonalphasetransitiontemperaturewas140K.Thefilms’excitonbindingenergywas77.6±10.9meVandtheenergyofopticalphononswas38.8±2.5meV.TheseresultssuggestthatperovskiteCH3NH3PbI3-xClxfilmshaveexcellentoptoelectroniccharacteristicswhichfurthersuggeststheirpotentialusageinperovskitebasedoptoelectronicdevices.

  • 标签: 金属卤化物 有机-无机 光致发光 钙钛矿 氧化锌 两步法
  • 简介:“微课”是指按照新课程标准及教学实践要求,以视频为主要载体,记录教师在课堂内外教育教学过程中围绕某个知识点(重点难点疑点)或教学环节而开展精彩教与学活动全过程.本文以“等差数列前n和”微课设计为例,谈谈其内容蕴意、教学创意和诗意感受.

  • 标签: 前N项和 等差数列 设计 教学实践 新课程标准 教学环节
  • 简介:、单项选择题(每小题5分,共50分)1.已知点(,-4),那么它到x轴距离为( )(A) (B)4 (C)- (D)52.如果k>b>0,那么直线y=kx+b图象必不经过( )(A)第象限 (B)第二象限(C)第三象限 (D)第四象限.函数y=kx图象经过点(-2,2),那么直线y=kx-k图象经过( )(A)第二、三、四象限 (B)第、二、三象限(C)第、二、四象限 (D)第、三、四象限4.满足b<0,c<0二次函数y=x2+bx+c图象大致是( )  5.两圆圆心都在y轴上,且两圆相交于A、B两点,若A点坐标为(2,2),则B点坐标为( )(A)(2,-2)

  • 标签: 二次函数 四象限 函数的图象 反比例函数 一次函数 取值范围
  • 简介:元选择题(每小题分,共45分)1.-|-2|倒数是( )(A)-2 (B)-12 (C)12 (D)22.(-a)2÷(-a)运算结果是( )(A)a6 (B)-a6 (C)a5 (D)-a53.如果个多边形内角和等于它外角和2倍,那么这个多边形是( )(A)三角形  (B)四边形(C)五边形  (D)六边形4.如果实数x、y满足|x+2|+(x-12y)2=0,那么xy值等于( )(A)-116 (B)116 (C)-18 (D)185.当锐角A>30°,cosA值( )(A)小于12 (B)小于32(C)大于12 (D)大于326.要使分式|x|-22x2-x-6

  • 标签: 综合训练 实数根 一次函数 延长线 取值范围 圆内接四边形
  • 简介:让M是紧缩orientable无法缩减3-manifold,和F是在把M切成二manifoldsM1和M2M必要连接关上表面。如果Mi有最小Heegaard切开Mi=$V_i\cup_{H_i}$V_i\cup_{H_i}有d(H1)Wi+d(H2)2(g(M1)+g(M2)?g(F))+1,然后g(M)=g(M1)+g(M2)?g(F)。

  • 标签: Heegaard分裂 流形 合并 不可约 表面 H2
  • 简介:TwopossiblereactionmechanismsofVS~+(~3∑~-,~1Γ)withCOinthegasphasehavebeenstudiedbyusingB3LYP/TZVPandCCSD(T)/6-311+G(3dr,3pd)methods:theO/Sexchangereaction(VS~++CO→VO~++CS)andtheS-transferreaction(VS~++CO→V~++COS).Thetworeactionsproceedviatwo-stepandone-stepmechanism,respectively.ThebarriersofthetripletandsingletPESsare30.6and50.9kcal/mol,respectively,forO/Sexchangereactionand7.3and50.2kcal/mol,respectively,fortheS-transferreaction.Theresultsindicatethatthetripletgroundstatereactionismorefavorable,andtheS-transferreactionismorefavorablethantheO/Sexchangereaction,whichisingoodagreementwiththeexperimentalobservation.

  • 标签: 钒元素 铅矿 硫化物 理论研究
  • 简介:Generally,ROSareregardedashostdefensemoleculesthatarereleasedbyneutrophilstodestroyexogenouspathogenssuchasbacteriaandtoactassecondarymessengersinsignaltransduction.However,increasedproductionofROSisalsoinvolvedininducingpathophysiologicalchangessuchasapoptosis,cellcycledisruption,andnecrosis.Forthisreason,inductionofROS-mediateddamageincancercellsbypharmacologicalagentsthateitherpromoteROSgenerationordisablethecellularantioxidantsystemisconsideredapotentialtherapeuticstrategyforpreferentiallykillingcancercells[1].

  • 标签: ROLE Redox STATUS
  • 简介:P1(G)是指这样图:G中所有k路作为P1(G)顶点集,两个不同顶点在Pk(G)中邻接当且仅当它们所对应两条k路并为G中(k+1)路或k圈,那么,完美图猜想对于路图P3(G)是成立

  • 标签: 顶点集 邻接 猜想 对应 成立 完美
  • 简介:TheinhomogeneityinacongrunetLiTaO3crystalhasbeenobservedbytransmissionsynchrotrontopography.ManyextraordinaryregionsexistincongruentLiTaO3crystalandtheyoftenshowdiffractionintensitydifferentfromthatofordinaryregionsinsynchrotrontopographs.DifferentialthermalanalysisindiatesthattheCurietemperatureoftheextraordinaryregionislowerthanthatofordinaryregion,andtheextraordinaryregionisreallyahighdefectdensityregion.Thediffractioncontrastoftheextraordinaryregioninsynchrotrontopographsisexplainedqualitativelybyacalculationattheselectedwavelength.2001PublishedbyElsevierScienceB.V.

  • 标签: LITAO3晶体 钽酸锂晶体 同步辐射形貌术 结构分析 X射线分析